Difference between revisions of "Sample Preparation for Joint 11-BM and 11-ID-B Measurements"

From Ug11bm
Jump to navigationJump to search
 
(9 intermediate revisions by the same user not shown)
Line 1: Line 1:
===Horizontal - Focused at Sample===
The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).
The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).


Contact beamline staff for full details on sample loading & capillary lengths before preparing your sample for complimentary measurements.
In the images below, the '''black colored'''  sections of capillary show where sample powder is required. <span style="color:red"><B>Red colored</b></span> sections show the location of epoxy or some similar substance to seal the capillary.  
 
[[Image:11IDB_holder2.png|frameless|300px| 11IDB_holder2]]


[[Image:11IDB_holder1.png|frameless|300px| 11IDB_holder1]]
These images show a capillary with a diameter =  0.0575" (1.46 mm). Contact beamline staff for full details on sample loading & capillary diameters and lengths before preparing your sample for complimentary measurements.


[[Image:11BM_holder2.png|frameless|300px| 11BM_holder2]]


[[Image:DuelMeasurmentCapillary.png|frameless|300px| DuelMeasurmentCapillary]]
[[Image:DuelMeasurmentCapillary.png|frameless|400px| DuelMeasurmentCapillary]]


[[image:SampleBase_Diagram.png|500px|Properly prepared sample for the 11-BM mail-in service]]
[[Image:11IDB_holder2.png|frameless|400px| 11IDB_holder2]]


[[Image:11IDB_holder1.png|frameless|400px| 11IDB_holder1]]


The following standard Cole-Parmer sizes are jointly compatible at 11-BM and 11-ID-B for  high throughput measurements.  
[[Image:11BM_holder2.png|frameless|400px| 11BM_holder2]]


Capillary ID size  x  OD size,            Cole-Parmer Part#,    Standard Size @ APS Beamlines
[[image:SampleBase_Diagram.png|400px|Properly prepared sample for the 11-BM mail-in service]]
0.0320" (0.81 mm)  x  0.0340" (0.86 mm),  # 95820-06,            @ 11-BM, 17-BM

Latest revision as of 02:16, 8 March 2013

The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).

In the images below, the black colored sections of capillary show where sample powder is required. Red colored sections show the location of epoxy or some similar substance to seal the capillary.

These images show a capillary with a diameter = 0.0575" (1.46 mm). Contact beamline staff for full details on sample loading & capillary diameters and lengths before preparing your sample for complimentary measurements.


DuelMeasurmentCapillary

11IDB_holder2

11IDB_holder1

11BM_holder2

Properly prepared sample for the 11-BM mail-in service