Difference between revisions of "Sample Preparation for Joint 11-BM and 11-ID-B Measurements"

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===Horizontal - Focused at Sample===
The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).


In the images below, the '''black colored'''  sections of capillary show where sample powder is required.  <span style="color:red"><B>Red colored</b></span> sections show the location of epoxy or some similar substance to seal the capillary.


The image below shows a burn of beam shape at the sample position beam with the tightest horizontal focus possible at the sample position.
These images show a capillary with a diameter =  0.0575" (1.46 mm). Contact beamline staff for full details on sample loading & capillary diameters and lengths before preparing your sample for complimentary measurements.


[[Image:11IDB_holder1.png|frameless|300px| 11IDB_holder1]]


[[Image:11IDB_holder2.png|frameless|300px| 11IDB_holder2]]
[[Image:DuelMeasurmentCapillary.png|frameless|400px| DuelMeasurmentCapillary]]


[[Image:11BM_holder1.png|frameless|300px| 11BM_holder1]]
[[Image:11IDB_holder2.png|frameless|400px| 11IDB_holder2]]


[[Image:11BM_holder2.png|frameless|300px| 11BM_holder2]]
[[Image:11IDB_holder1.png|frameless|400px| 11IDB_holder1]]


[[Image:DuelMeasurmentCapillary.png|frameless|300px| DuelMeasurmentCapillary]
[[Image:11BM_holder2.png|frameless|400px| 11BM_holder2]]


[[image:SampleBase_Diagram.png|500px|Properly prepared sample for the 11-BM mail-in service]]
[[image:SampleBase_Diagram.png|400px|Properly prepared sample for the 11-BM mail-in service]]
 
 
Users anticipating performing complimentary scattering measurements on a single sample at other APS powder beamlines should consider using the following standard Cole-Parmer sizes. These are compatible with samples holders at the beamlines noted below. However, it is also important to contact beamline staff for details on sample loading & capillary lengths before preparing your sample for complimentary measurements.
Capillary ID size  x  OD size,            Cole-Parmer Part#,    Standard Size @ APS Beamlines
0.0320" (0.81 mm)  x  0.0340" (0.86 mm),  # 95820-06,            @ 11-BM, 17-BM

Latest revision as of 02:16, 8 March 2013

The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).

In the images below, the black colored sections of capillary show where sample powder is required. Red colored sections show the location of epoxy or some similar substance to seal the capillary.

These images show a capillary with a diameter = 0.0575" (1.46 mm). Contact beamline staff for full details on sample loading & capillary diameters and lengths before preparing your sample for complimentary measurements.


DuelMeasurmentCapillary

11IDB_holder2

11IDB_holder1

11BM_holder2

Properly prepared sample for the 11-BM mail-in service

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