Difference between revisions of "Sample Preparation for Joint 11-BM and 11-ID-B Measurements"

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===Horizontal - Focused at Sample===
===Horizontal - Focused at Sample===


The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).


The image below shows a burn of beam shape at the sample position beam with the tightest horizontal focus possible at the sample position.
Contact beamline staff for full details on sample loading & capillary lengths before preparing your sample for complimentary measurements.


[[Image:11IDB_holder2.png|frameless|300px| 11IDB_holder2]]
[[Image:11IDB_holder2.png|frameless|300px| 11IDB_holder2]]


[[Image:11IDB_holder1.png|frameless|300px| 11IDB_holder1]]
[[Image:11IDB_holder1.png|frameless|300px| 11IDB_holder1]]
[[Image:11BM_holder1.png|frameless|300px| 11BM_holder1]]


[[Image:11BM_holder2.png|frameless|300px| 11BM_holder2]]
[[Image:11BM_holder2.png|frameless|300px| 11BM_holder2]]
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Users anticipating performing complimentary scattering measurements on a single sample at other APS powder beamlines should consider using the following standard Cole-Parmer sizes. These are compatible with samples holders at the beamlines noted below. However, it is also important to contact beamline staff for details on sample loading & capillary lengths before preparing your sample for complimentary measurements.
The following standard Cole-Parmer sizes are jointly compatible at 11-BM and 11-ID-B for high throughput measurements.  
 
Capillary ID size  x  OD size,            Cole-Parmer Part#,    Standard Size @ APS Beamlines
Capillary ID size  x  OD size,            Cole-Parmer Part#,    Standard Size @ APS Beamlines
0.0320" (0.81 mm)  x  0.0340" (0.86 mm),  # 95820-06,            @ 11-BM, 17-BM
0.0320" (0.81 mm)  x  0.0340" (0.86 mm),  # 95820-06,            @ 11-BM, 17-BM

Revision as of 01:43, 5 March 2013

Horizontal - Focused at Sample

The images below show how a capillary could be prepared for complimentary scattering measurements to be compatible with high throughput sample holders at both beamlines 11-BM (robot loading) and 11-ID-B (linear sample cassette).

Contact beamline staff for full details on sample loading & capillary lengths before preparing your sample for complimentary measurements.

11IDB_holder2

11IDB_holder1

11BM_holder2

DuelMeasurmentCapillary

Properly prepared sample for the 11-BM mail-in service


The following standard Cole-Parmer sizes are jointly compatible at 11-BM and 11-ID-B for high throughput measurements.

Capillary ID size x OD size, Cole-Parmer Part#, Standard Size @ APS Beamlines 0.0320" (0.81 mm) x 0.0340" (0.86 mm), # 95820-06, @ 11-BM, 17-BM