Difference between revisions of "Main Page"

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This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
== [[11-BM News]] ==
Archived [https://wiki-ext.aps.anl.gov/ug11bm/index.php/11-BM_News news and updates] about 11-BM and powder diffraction at the APS


== Safety & Training ==
== Safety & Training ==
APS Safety & Training Links:
APS Safety & Training Links:
http://www.aps.anl.gov/Safety_and_Training/
https://www.aps.anl.gov/Safety-and-Training/
 
XSD division Safety & Training Links:
http://www.aps.anl.gov/Xray_Science_Division/Safety/


Experiment Safety Approval Forms (ESAFs):
Experiment Safety Approval Forms (ESAFs):
http://www.aps.anl.gov/Safety_and_Training/Experiment_Safety_Approval_Form/index.html
https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page


Experiment Hazard Classes
Experiment Hazard Classes
http://www.aps.anl.gov/Safety_and_Training/Experiment_Hazard_Classes/index.html
https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions
 
User Policies in APS Central Documents:
http://centraldocs.aps.anl.gov/policy_procedures/user/
 
APS-IT Emergency Line
dial 2-9700 to report and or listen to a status message about major IT system and network outages
 


== Sample Preparation ==
== Sample Preparation ==
''under construction''
* [[Mail-In Powder Diffraction Measurements]]
* [[Mail-In Powder Diffraction Measurements]]
* [[Using Glass or Fused Quartz Capillaries]]
* [[X-ray Absorption and Fluorescence]]
* [[X-ray Absorption and Fluorescence]]
* [[Samples with Strong X-Ray Absorption]]
* [[Samples with Strong X-Ray Absorption]]
 
* [[Air Sensitive Samples]]
* [[Using Glass or Fused Quartz Capillaries]]
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]]
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]]
 
* [[Modifying Mail-In Sample Bases]]
* [[Air Sensitive Samples]]
 
* [[On-Site Experiments]]
* [[On-Site Experiments]]
* [[Supplies and Tools]]
* [[Supplies and Tools]]
**[http://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries]
**[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries]
 
* [[Hazards]]
* [[Hazards]]
* [[Videos]]
* [[Videos]]
----
old links
[[Equipment and Tools]]
[[X-ray absorption & fluorescence]]
[[Capillary Tubes]]
Mail-In Sample Prep Notes [http://11bm.xor.aps.anl.gov/users_prep.html @ 11-BM Webpage] or as [http://11bm.xor.aps.anl.gov/documents/11BM_MailInUserInstructions_(BaseShipmentVersion)_Jan2011.pdf .pdf download]
[[Sample Preparation Gallery]]
[http://11bm.xor.aps.anl.gov/documents/11BM_SamplePrepNestedCapillaryKapton.pdf Notes for Sample Prep with Nested Capillaries in Kapton (.pdf download)]
[[Powder Sieves]]
[[Useful Sample Prep Tools]]
[[Nesting Capillaries in Kapton Tubes]]
== Beamline Controls ==
* [[Sample Robot]]
== Data Collection ==
===Instrumental Background (No sample)===
see 11BM webpage for more info:
http://11bm.xor.aps.anl.gov/standards_data.html
Plot of background for empty 11-BM 0.8 mm Kapton capillary (@ 30 KeV)
http://11bm.xor.aps.anl.gov/data/standards/Kapton/2010_1/11BM_Kapton.jpg
Plot of empty background (no sample or capillary)for 11-BM, air scatter only (@ 30 KeV)
http://11bm.xor.aps.anl.gov/data/standards/background/11BM_background_air_scatter.jpg


== Software ==
== Software ==


=== Data Collection/Processing ===
=== Data Collection/Processing ===
*[http://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)]
*[https://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)]
* [http://11bm.xor.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption]
* [https://11bm.xray.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption]
* [[Calibration]]
* [[Calibration]]
* [[Merge]]
* [[Merge]]
* [[Off-Site Merge]]
* [[Off-Site Merge]]
* Background: see [[Standards Data]]


=== On-Site Users: Beamline Controls===
=== On-Site Users: Beamline Controls===
* [[MEDM Status Displays]]
* [[MEDM Status Displays]]
* [[UserControl]]
* [[UserControl]]
* [[Sample_Robot]]


=== Data Analysis ===
=== Data Analysis ===
* [http://11bm.xor.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS]   
* [https://11bm.xray.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS]   
* [https://subversion.xor.aps.anl.gov/trac/pyGSAS GSAS-II]
* [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II]
* [http://11bm.xray.aps.anl.gov/cmpr.html CMPR]
* [https://11bm.xray.aps.anl.gov/cmpr.html CMPR]
 


== [[Sample Environments]] ==
== [[Sample Environments]] ==
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pages for more information on specific environments
pages for more information on specific environments


* [[Oxford Helium Cryostat]]
* [[Oxford Helium Cryostat]]  
* [[Hot Gas Blower (Cyberstar)]]
* [[Hot Gas Blower (Cyberstar)]]
* [[Gas Handling Equipment]]
* [[Gas Handling Equipment]]
* [[Resistive Heating Furnace]]


 
== Other Equipment ==
 
== [[Other Equipment]] ==
Temperature Controls, Power Supplies etc
Temperature Controls, Power Supplies etc
 
*[[TEXIO PD18-30AD DC Power Supply]]
*[[SRS PTC10 Temperature Controller]]
*[[KI Flow Meters]]  (for B-hutch Gas Patch Panel)
*[[Goniometer Head Alignment Rig]]


== Status & History ==
== Status & History ==
'''11-BM Status Page'''   
'''11-BM Status Page'''   
http://11bm.xor.aps.anl.gov/status/status.html
https://11bm.xray.aps.anl.gov/status/status.html


APS Ring Status   
APS Ring Status   
http://www.aps.anl.gov/Facility/Status/
https://www.aps.anl.gov/Facility/Status/


* [[11-BM Parameter Log]]
* [[11-BM Parameter Log]]
Line 129: Line 78:


* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]
* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]


== Video Webcams & Monitors ==
== Video Webcams & Monitors ==
* [http://11bmcam.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted)]
* [https://11bmcam.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted and only viewable onsite)]
* [http://11bmcam2.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted)]
* [https://11bmcam2.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted and only viewable onsite)]
* [http://axis.xor.aps.anl.gov/view/index.shtml 11BM Video Server]
* [https://axis.xray.aps.anl.gov/view/index.shtml 11BM Video Server]
* [http://11bm.xor.aps.anl.gov/status/livedata.html 11BM Live Data]
* [https://11bm.xray.aps.anl.gov/status/livedata.html 11BM Live Data]


== 11-BM Rapid Acces ==  
== 11-BM Rapid Access ==  
http://11bm.xray.aps.anl.gov/instructions.html
*[[Rapid Access Instructions]]: for mail-in program
*[[Mail-In Bases]]: for mail-in program


== Standards Data ==
== Standards Data ==
standards reference powder diffraction data
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data Standards Data]:
reference powder diffraction data for standard (SRM) samples, plus example fits


http://11bm.xray.aps.anl.gov/standards_data.html
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data#Instrument_Parameter_and_Input_Files Instrument Parameter and Input Files]:
instrument parameter and input information


== 11-BM, APS & ANL Links ==
== 11-BM, APS & ANL Links ==
11-BM Homepage
*11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html  
http://11bm.xor.aps.anl.gov/home.html  
 
* APS powder diffraction overview sheet [https://11bm.xray.aps.anl.gov/documents/APS_PowderXRD_Flyer_Oct2012.pdf download .pdf]


SRS Group (Sector 11) Homepage
*SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/
http://www.aps.anl.gov/Xray_Science_Division/Structural_Science/


APS Beam Status & History
*APS Beam Status & History:  https://www.aps.anl.gov/Facility/Status/
http://www.aps.anl.gov/Facility/Status/


GUP, ESAF & APS Training links
*GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/
http://www.aps.anl.gov/Users/Current/


APS Beamline Phone Directory
*APS New User Registration: https://www.aps.anl.gov/Users/New/ (see [[User Registration Notes]])
http://www.aps.anl.gov/Beamlines/Phone_Directory/


* [http://www.aps.anl.gov/Users/Contacts/ APS Contacts]
*[[Industrial and Proprietary Users]]
* [http://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]


* [http://www.aim.anl.gov/ Argonne Library (internal only)]
*APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/


* [http://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
* [https://www.aps.anl.gov/Users/Contacts/ APS Contacts]
* [http://www.anlgh.org/anlghhome.html Argonne Guest House]
* [https://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]
* [https://maps.anl.gov/ Interactive Argonne Campus Map]


* [[Local Dining Options]]
* [https://www.aim.anl.gov/  Argonne Library (internal only)]


====On-Site Accommodation & Dining====
*[[Off-Site Local Dining Options]]
*[https://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
*[https://www.anlgh.org/anlghhome.html Argonne Guest House]


== Assorted Links ==
== Assorted Links ==
Line 180: Line 132:


* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]
* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]


== Software Notes ==
== Software Notes ==
Line 187: Line 138:
* [[GSAS Refinement Hints]]
* [[GSAS Refinement Hints]]
* [[Preferred orientation in EXPGUI/GSAS]]
* [[Preferred orientation in EXPGUI/GSAS]]
* [[Combined X-Ray and Neutron Refinements]]
* [[CMPR]]
* [[CMPR]]

Latest revision as of 18:48, 22 April 2020

User Wiki for APS Beamline 11-BM

This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.

11-BM News

Archived news and updates about 11-BM and powder diffraction at the APS

Safety & Training

APS Safety & Training Links: https://www.aps.anl.gov/Safety-and-Training/

Experiment Safety Approval Forms (ESAFs): https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page

Experiment Hazard Classes https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions

Sample Preparation

Software

Data Collection/Processing

On-Site Users: Beamline Controls

Data Analysis

Sample Environments

pages for more information on specific environments

Other Equipment

Temperature Controls, Power Supplies etc

Status & History

11-BM Status Page https://11bm.xray.aps.anl.gov/status/status.html

APS Ring Status https://www.aps.anl.gov/Facility/Status/

Video Webcams & Monitors

11-BM Rapid Access

Standards Data

Standards Data: reference powder diffraction data for standard (SRM) samples, plus example fits

Instrument Parameter and Input Files: instrument parameter and input information

11-BM, APS & ANL Links

On-Site Accommodation & Dining

Assorted Links

Software Notes

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