Difference between revisions of "Main Page"
(45 intermediate revisions by the same user not shown) | |||
Line 2: | Line 2: | ||
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically. | This wiki contains information for users of the APS beamline 11-BM; new content is added periodically. | ||
== [[11-BM News]] == | |||
Archived [https://wiki-ext.aps.anl.gov/ug11bm/index.php/11-BM_News news and updates] about 11-BM and powder diffraction at the APS | |||
== Safety & Training == | == Safety & Training == | ||
APS Safety & Training Links: | APS Safety & Training Links: | ||
https://www.aps.anl.gov/Safety-and-Training/ | |||
Experiment Safety Approval Forms (ESAFs): | Experiment Safety Approval Forms (ESAFs): | ||
https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page | |||
Experiment Hazard Classes | Experiment Hazard Classes | ||
https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions | |||
== Sample Preparation == | == Sample Preparation == | ||
Line 29: | Line 23: | ||
* [[Using Glass or Fused Quartz Capillaries]] | * [[Using Glass or Fused Quartz Capillaries]] | ||
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]] | * [[Nesting Glass/Quartz Capillaries in Kapton Tubes]] | ||
* [[Modifying Mail-In Sample Bases]] | |||
* [[On-Site Experiments]] | * [[On-Site Experiments]] | ||
* [[Supplies and Tools]] | * [[Supplies and Tools]] | ||
**[ | **[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries] | ||
* [[Hazards]] | * [[Hazards]] | ||
* [[Videos]] | * [[Videos]] | ||
Line 38: | Line 33: | ||
=== Data Collection/Processing === | === Data Collection/Processing === | ||
*[ | *[https://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)] | ||
* [ | * [https://11bm.xray.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption] | ||
* [[Calibration]] | * [[Calibration]] | ||
* [[Merge]] | * [[Merge]] | ||
Line 51: | Line 46: | ||
=== Data Analysis === | === Data Analysis === | ||
* [ | * [https://11bm.xray.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS] | ||
* [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II] | * [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II] | ||
* [ | * [https://11bm.xray.aps.anl.gov/cmpr.html CMPR] | ||
== [[Sample Environments]] == | == [[Sample Environments]] == | ||
Line 59: | Line 54: | ||
pages for more information on specific environments | pages for more information on specific environments | ||
* [[Oxford Helium Cryostat]] | * [[Oxford Helium Cryostat]] | ||
* [[Hot Gas Blower (Cyberstar)]] | * [[Hot Gas Blower (Cyberstar)]] | ||
* [[Gas Handling Equipment]] | * [[Gas Handling Equipment]] | ||
* [[Resistive Heating Furnace]] | |||
== | == Other Equipment == | ||
Temperature Controls, Power Supplies etc | Temperature Controls, Power Supplies etc | ||
*[[TEXIO PD18-30AD DC Power Supply]] | |||
*[[SRS PTC10 Temperature Controller]] | |||
*[[KI Flow Meters]] (for B-hutch Gas Patch Panel) | |||
*[[Goniometer Head Alignment Rig]] | |||
== Status & History == | == Status & History == | ||
'''11-BM Status Page''' | '''11-BM Status Page''' | ||
https://11bm.xray.aps.anl.gov/status/status.html | |||
APS Ring Status | APS Ring Status | ||
https://www.aps.anl.gov/Facility/Status/ | |||
* [[11-BM Parameter Log]] | * [[11-BM Parameter Log]] | ||
Line 81: | Line 80: | ||
== Video Webcams & Monitors == | == Video Webcams & Monitors == | ||
* [ | * [https://11bmcam.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted and only viewable onsite)] | ||
* [ | * [https://11bmcam2.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted and only viewable onsite)] | ||
* [ | * [https://axis.xray.aps.anl.gov/view/index.shtml 11BM Video Server] | ||
* [ | * [https://11bm.xray.aps.anl.gov/status/livedata.html 11BM Live Data] | ||
== 11-BM Rapid Access == | == 11-BM Rapid Access == | ||
[[Rapid Access Instructions]]: for mail-in program | *[[Rapid Access Instructions]]: for mail-in program | ||
*[[Mail-In Bases]]: for mail-in program | |||
== Standards Data == | == Standards Data == | ||
[ | [https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data Standards Data]: | ||
reference powder diffraction data for standard (SRM) samples, plus example fits | |||
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data#Instrument_Parameter_and_Input_Files Instrument Parameter and Input Files]: | |||
instrument parameter and input information | |||
== 11-BM, APS & ANL Links == | == 11-BM, APS & ANL Links == | ||
*11-BM Homepage: | *11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html | ||
* APS powder diffraction overview sheet [https://11bm.xray.aps.anl.gov/documents/APS_PowderXRD_Flyer_Oct2012.pdf download .pdf] | |||
*SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/ | |||
* | *APS Beam Status & History: https://www.aps.anl.gov/Facility/Status/ | ||
*APS | *GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/ | ||
* | *APS New User Registration: https://www.aps.anl.gov/Users/New/ (see [[User Registration Notes]]) | ||
* | *[[Industrial and Proprietary Users]] | ||
*APS Beamline Phone Directory | *APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/ | ||
* [ | * [https://www.aps.anl.gov/Users/Contacts/ APS Contacts] | ||
* [ | * [https://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links] | ||
* [https://maps.anl.gov/ Interactive Argonne Campus Map] | |||
* [ | * [https://www.aim.anl.gov/ Argonne Library (internal only)] | ||
====On-Site Accommodation & Dining==== | |||
[[Off-Site Local Dining Options]] | *[[Off-Site Local Dining Options]] | ||
[ | *[https://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill] | ||
[ | *[https://www.anlgh.org/anlghhome.html Argonne Guest House] | ||
== Assorted Links == | == Assorted Links == | ||
* [[NIST SRM Certificates]] | * [[NIST SRM Certificates]] | ||
* [[11BM Calibration Sample: Lattice & Atomic Position Values]] | |||
* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel] | |||
* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)] | |||
== Software Notes == | == Software Notes == | ||
Line 130: | Line 138: | ||
* [[GSAS Refinement Hints]] | * [[GSAS Refinement Hints]] | ||
* [[Preferred orientation in EXPGUI/GSAS]] | * [[Preferred orientation in EXPGUI/GSAS]] | ||
* [[Combined X-Ray and Neutron Refinements]] | |||
* [[CMPR]] | * [[CMPR]] |
Latest revision as of 18:48, 22 April 2020
User Wiki for APS Beamline 11-BM
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
11-BM News
Archived news and updates about 11-BM and powder diffraction at the APS
Safety & Training
APS Safety & Training Links: https://www.aps.anl.gov/Safety-and-Training/
Experiment Safety Approval Forms (ESAFs): https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page
Experiment Hazard Classes https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions
Sample Preparation
- Mail-In Powder Diffraction Measurements
- X-ray Absorption and Fluorescence
- Samples with Strong X-Ray Absorption
- Air Sensitive Samples
- Using Glass or Fused Quartz Capillaries
- Nesting Glass/Quartz Capillaries in Kapton Tubes
- Modifying Mail-In Sample Bases
- On-Site Experiments
- Supplies and Tools
- Hazards
- Videos
Software
Data Collection/Processing
- 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)
- Absorb: compute x-ray absorption
- Calibration
- Merge
- Off-Site Merge
- Background: see Standards Data
On-Site Users: Beamline Controls
Data Analysis
Sample Environments
pages for more information on specific environments
Other Equipment
Temperature Controls, Power Supplies etc
- TEXIO PD18-30AD DC Power Supply
- SRS PTC10 Temperature Controller
- KI Flow Meters (for B-hutch Gas Patch Panel)
- Goniometer Head Alignment Rig
Status & History
11-BM Status Page https://11bm.xray.aps.anl.gov/status/status.html
APS Ring Status https://www.aps.anl.gov/Facility/Status/
Video Webcams & Monitors
- 11BM Web Camera:Side View (restricted and only viewable onsite)
- 11BM Web Camera:Beam Path View (restricted and only viewable onsite)
- 11BM Video Server
- 11BM Live Data
11-BM Rapid Access
- Rapid Access Instructions: for mail-in program
- Mail-In Bases: for mail-in program
Standards Data
Standards Data: reference powder diffraction data for standard (SRM) samples, plus example fits
Instrument Parameter and Input Files: instrument parameter and input information
11-BM, APS & ANL Links
- 11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html
- APS powder diffraction overview sheet download .pdf
- SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/
- APS Beam Status & History: https://www.aps.anl.gov/Facility/Status/
- GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/
- APS New User Registration: https://www.aps.anl.gov/Users/New/ (see User Registration Notes)
- APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/