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'''11-BM | '''User Wiki for APS Beamline 11-BM''' | ||
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically. | |||
== [[11-BM News]] == | |||
Archived [https://wiki-ext.aps.anl.gov/ug11bm/index.php/11-BM_News news and updates] about 11-BM and powder diffraction at the APS | |||
== Safety & Training == | |||
APS Safety & Training Links: | |||
https://www.aps.anl.gov/Safety-and-Training/ | |||
Experiment Safety Approval Forms (ESAFs): | |||
https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page | |||
Experiment Hazard Classes | |||
https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions | |||
== Data Processing == | == Sample Preparation == | ||
* [[Mail-In Powder Diffraction Measurements]] | |||
* [[X-ray Absorption and Fluorescence]] | |||
* [[Samples with Strong X-Ray Absorption]] | |||
* [[Air Sensitive Samples]] | |||
* [[Using Glass or Fused Quartz Capillaries]] | |||
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]] | |||
* [[Modifying Mail-In Sample Bases]] | |||
* [[On-Site Experiments]] | |||
* [[Supplies and Tools]] | |||
**[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries] | |||
* [[Hazards]] | |||
* [[Videos]] | |||
== Software == | |||
=== Data Collection/Processing === | |||
*[https://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)] | |||
* [https://11bm.xray.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption] | |||
* [[Calibration]] | * [[Calibration]] | ||
* [[Merge]] | * [[Merge]] | ||
* [[Off-Site Merge]] | |||
* Background: see [[Standards Data]] | |||
=== On-Site Users: Beamline Controls=== | |||
* [[MEDM Status Displays]] | |||
* [[UserControl]] | |||
* [[Sample_Robot]] | |||
=== Data Analysis === | |||
* [https://11bm.xray.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS] | |||
* [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II] | |||
* [https://11bm.xray.aps.anl.gov/cmpr.html CMPR] | |||
== [[Sample Environments]] == | |||
pages for more information on specific environments | |||
* [[Oxford Helium Cryostat]] | |||
* [[Hot Gas Blower (Cyberstar)]] | |||
* [[Gas Handling Equipment]] | |||
* [[Resistive Heating Furnace]] | |||
== | == Other Equipment == | ||
* [[ | Temperature Controls, Power Supplies etc | ||
*[[TEXIO PD18-30AD DC Power Supply]] | |||
*[[SRS PTC10 Temperature Controller]] | |||
*[[KI Flow Meters]] (for B-hutch Gas Patch Panel) | |||
*[[Goniometer Head Alignment Rig]] | |||
== Status & History == | |||
'''11-BM Status Page''' | |||
https://11bm.xray.aps.anl.gov/status/status.html | |||
APS Ring Status | |||
https://www.aps.anl.gov/Facility/Status/ | |||
* [[11-BM Parameter Log]] | |||
* [http://twitter.com/#!/aps_notify APS Twitter Beam Status Feed] | |||
* [http://twitter.com/#!/APS_11BM/ 11BM Twitter Beam Status Feed] | |||
== Video Webcams & Monitors == | |||
* [https://11bmcam.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted and only viewable onsite)] | |||
* [https://11bmcam2.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted and only viewable onsite)] | |||
* [https://axis.xray.aps.anl.gov/view/index.shtml 11BM Video Server] | |||
* [https://11bm.xray.aps.anl.gov/status/livedata.html 11BM Live Data] | |||
== 11-BM Rapid Access == | |||
*[[Rapid Access Instructions]]: for mail-in program | |||
*[[Mail-In Bases]]: for mail-in program | |||
== Standards Data == | |||
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data Standards Data]: | |||
reference powder diffraction data for standard (SRM) samples, plus example fits | |||
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data#Instrument_Parameter_and_Input_Files Instrument Parameter and Input Files]: | |||
instrument parameter and input information | |||
== 11-BM, APS & ANL Links == | |||
*11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html | |||
* APS powder diffraction overview sheet [https://11bm.xray.aps.anl.gov/documents/APS_PowderXRD_Flyer_Oct2012.pdf download .pdf] | |||
*SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/ | |||
*APS Beam Status & History: https://www.aps.anl.gov/Facility/Status/ | |||
*GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/ | |||
*APS New User Registration: https://www.aps.anl.gov/Users/New/ (see [[User Registration Notes]]) | |||
*[[Industrial and Proprietary Users]] | |||
*APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/ | |||
* [https://www.aps.anl.gov/Users/Contacts/ APS Contacts] | |||
* [https://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links] | |||
* [https://maps.anl.gov/ Interactive Argonne Campus Map] | |||
* [https://www.aim.anl.gov/ Argonne Library (internal only)] | |||
* [ | |||
* [ | ====On-Site Accommodation & Dining==== | ||
* [ | *[[Off-Site Local Dining Options]] | ||
* [ | *[https://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill] | ||
*[https://www.anlgh.org/anlghhome.html Argonne Guest House] | |||
* [ | == Assorted Links == | ||
* [[NIST SRM Certificates]] | |||
* [ | * [[11BM Calibration Sample: Lattice & Atomic Position Values]] | ||
* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel] | |||
* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)] | |||
* [ | == Software Notes == | ||
* [ | * [[GSAS Profile Terms]] | ||
* [ | * [[Sequential GSAS]] | ||
* [[GSAS Refinement Hints]] | |||
* [[Preferred orientation in EXPGUI/GSAS]] | |||
* [[Combined X-Ray and Neutron Refinements]] | |||
* [[CMPR]] |
Latest revision as of 18:48, 22 April 2020
User Wiki for APS Beamline 11-BM
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
11-BM News
Archived news and updates about 11-BM and powder diffraction at the APS
Safety & Training
APS Safety & Training Links: https://www.aps.anl.gov/Safety-and-Training/
Experiment Safety Approval Forms (ESAFs): https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page
Experiment Hazard Classes https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions
Sample Preparation
- Mail-In Powder Diffraction Measurements
- X-ray Absorption and Fluorescence
- Samples with Strong X-Ray Absorption
- Air Sensitive Samples
- Using Glass or Fused Quartz Capillaries
- Nesting Glass/Quartz Capillaries in Kapton Tubes
- Modifying Mail-In Sample Bases
- On-Site Experiments
- Supplies and Tools
- Hazards
- Videos
Software
Data Collection/Processing
- 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)
- Absorb: compute x-ray absorption
- Calibration
- Merge
- Off-Site Merge
- Background: see Standards Data
On-Site Users: Beamline Controls
Data Analysis
Sample Environments
pages for more information on specific environments
Other Equipment
Temperature Controls, Power Supplies etc
- TEXIO PD18-30AD DC Power Supply
- SRS PTC10 Temperature Controller
- KI Flow Meters (for B-hutch Gas Patch Panel)
- Goniometer Head Alignment Rig
Status & History
11-BM Status Page https://11bm.xray.aps.anl.gov/status/status.html
APS Ring Status https://www.aps.anl.gov/Facility/Status/
Video Webcams & Monitors
- 11BM Web Camera:Side View (restricted and only viewable onsite)
- 11BM Web Camera:Beam Path View (restricted and only viewable onsite)
- 11BM Video Server
- 11BM Live Data
11-BM Rapid Access
- Rapid Access Instructions: for mail-in program
- Mail-In Bases: for mail-in program
Standards Data
Standards Data: reference powder diffraction data for standard (SRM) samples, plus example fits
Instrument Parameter and Input Files: instrument parameter and input information
11-BM, APS & ANL Links
- 11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html
- APS powder diffraction overview sheet download .pdf
- SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/
- APS Beam Status & History: https://www.aps.anl.gov/Facility/Status/
- GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/
- APS New User Registration: https://www.aps.anl.gov/Users/New/ (see User Registration Notes)
- APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/