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'''11-BM User Wiki'''
'''User Wiki for APS Beamline 11-BM'''


This wiki contains information for on-site users of the APS beamline 11-BM.  New content will be added with time.
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.


== Sample Preparation ==
== [[11-BM News]] ==
Archived [https://wiki-ext.aps.anl.gov/ug11bm/index.php/11-BM_News news and updates] about 11-BM and powder diffraction at the APS


* [https://subversion.xor.aps.anl.gov/11BMweb/External/trunk/documents/11BM_SamplePrepNestedCapillaryKapton.pdf Notes for Sample Prep with Nested Capillaries in Kapton (.pdf download)]
== Safety & Training ==
APS Safety & Training Links:
https://www.aps.anl.gov/Safety-and-Training/


* Mail-In Sample Prep Notes [http://11bm.xor.aps.anl.gov/users_prep.html @ 11-BM Webpage] or as [http://11bm.xor.aps.anl.gov/documents/11BM_MailInUserInstructions_(BaseShipmentVersion)_Jan2011.pdf .pdf download]
Experiment Safety Approval Forms (ESAFs):
https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page


*[[Sample Preparation Gallery]]
Experiment Hazard Classes
https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions


== Sample Preparation ==
* [[Mail-In Powder Diffraction Measurements]]
* [[X-ray Absorption and Fluorescence]]
* [[Samples with Strong X-Ray Absorption]]
* [[Air Sensitive Samples]]
* [[Using Glass or Fused Quartz Capillaries]]
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]]
* [[Modifying Mail-In Sample Bases]]
* [[On-Site Experiments]]
* [[Supplies and Tools]]
**[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries]
* [[Hazards]]
* [[Videos]]


* [http://11bm.xor.aps.anl.gov/absorb/absorb.php '''Absorb''': compute X-ray absorption for powder XRD capillary samples (11BM page)]
== Software ==


* [http://csrri.iit.edu/mucal.html '''MuCal''': calculate X-ray absorption, fluorescence and more (by C. Segre @ IIT/ANL)]
=== Data Collection/Processing ===
*[https://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)]
* [https://11bm.xray.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption]
* [[Calibration]]
* [[Merge]]
* [[Off-Site Merge]]
* Background: see [[Standards Data]]  


== Beamline Controls ==
=== On-Site Users: Beamline Controls===
* [[MEDM Status Displays]]
* [[MEDM Status Displays]]
* [[UserControl]]
* [[UserControl]]
* [[Sample_Robot]]
=== Data Analysis ===
* [https://11bm.xray.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS] 
* [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II]
* [https://11bm.xray.aps.anl.gov/cmpr.html CMPR]


== Data Processing ==
== [[Sample Environments]] ==
* [[Calibration]]
 
* [[Merge]]
pages for more information on specific environments
* [[Off-Site Merge]]
 
* [[Oxford Helium Cryostat]]
* [[Hot Gas Blower (Cyberstar)]]
* [[Gas Handling Equipment]]
* [[Resistive Heating Furnace]]


== Equipment ==
== Other Equipment ==
* [[Oxford Helium Cryostat]]
Temperature Controls, Power Supplies etc
* [[N2 Cyrostream]]
*[[TEXIO PD18-30AD DC Power Supply]]
* [[Hot Gas Blower]]
*[[SRS PTC10 Temperature Controller]]
* [[Red Goniometer Spinner/Oscillation Stage ]]
*[[KI Flow Meters]] (for B-hutch Gas Patch Panel)
*[[Goniometer Head Alignment Rig]]


== Status & History ==
== Status & History ==
'''11-BM Status Page''' 
https://11bm.xray.aps.anl.gov/status/status.html


* [http://11bm.xor.aps.anl.gov/status/status.html '''11-BM Status Page''']
APS Ring Status
 
https://www.aps.anl.gov/Facility/Status/
* [http://www.aps.anl.gov/Facility/Status/ APS Ring Status]


* [[11-BM Parameter Log]]
* [[11-BM Parameter Log]]
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* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]
* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]


== Video Webcams & Monitors ==
* [https://11bmcam.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted and only viewable onsite)]
* [https://11bmcam2.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted and only viewable onsite)]
* [https://axis.xray.aps.anl.gov/view/index.shtml 11BM Video Server]
* [https://11bm.xray.aps.anl.gov/status/livedata.html 11BM Live Data]
== 11-BM Rapid Access ==
*[[Rapid Access Instructions]]: for mail-in program
*[[Mail-In Bases]]: for mail-in program
== Standards Data ==
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data Standards Data]:
reference powder diffraction data for standard (SRM) samples, plus example fits
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data#Instrument_Parameter_and_Input_Files Instrument Parameter and Input Files]:
instrument parameter and input information


== 11-BM, APS & ANL Links ==
*11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html


== Video Webcams & Monitors ==
* APS powder diffraction overview sheet [https://11bm.xray.aps.anl.gov/documents/APS_PowderXRD_Flyer_Oct2012.pdf download .pdf]
* [http://11bmcam.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted)]
 
* [http://11bmcam2.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted)]
*SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/
* [http://axis.xor.aps.anl.gov/view/index.shtml 11BM Video Server]
* [http://11bm.xor.aps.anl.gov/status/livedata.html 11BM Live Data]


== Useful APS & ANL Links ==
*APS Beam Status & History: https://www.aps.anl.gov/Facility/Status/
* [http://11bm.xor.aps.anl.gov/home.html 11-BM Homepage]
* [http://www.aps.anl.gov/Xray_Science_Division/Structural_Science/ SRS Group (Sector 11) Homepage]


* [http://www.aps.anl.gov/Facility/Status/ Beam Status & History]
*GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/
* [http://www.aps.anl.gov/Users/Current/ GUP, ESAF & APS Training links]


* [http://www.aps.anl.gov/Beamlines/Phone_Directory/ APS Beamline Phone Numbers]
*APS New User Registration: https://www.aps.anl.gov/Users/New/ (see [[User Registration Notes]])
* [http://www.aps.anl.gov/Users/Contacts/ APS Contacts]
* [http://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]


* [http://www.aim.anl.gov/  Argonne Library (internal only)]
*[[Industrial and Proprietary Users]]


* [http://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
*APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/
* [http://www.anlgh.org/anlghhome.html Argonne Guest House]


* [https://www.aps.anl.gov/Users/Contacts/ APS Contacts]
* [https://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]
* [https://maps.anl.gov/ Interactive Argonne Campus Map]


* [[Local Dining Options]]
* [https://www.aim.anl.gov/  Argonne Library (internal only)]


====On-Site Accommodation & Dining====
*[[Off-Site Local Dining Options]]
*[https://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
*[https://www.anlgh.org/anlghhome.html Argonne Guest House]


== Assorted Other Stuff ==
== Assorted Links ==
* [[NIST SRM Certificates]]  
* [[NIST SRM Certificates]]  
* [[11BM Calibration Sample: Lattice & Atomic Position Values]]


* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel]
* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel]


* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]
* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]


== GSAS/EXPGUI Notes ==
== Software Notes ==
* [[GSAS Profile Terms]]
* [[Sequential GSAS]]
* [[Sequential GSAS]]
* [[GSAS Refinement Hints]]
* [[GSAS Refinement Hints]]
* [[Preferred orientation in EXPGUI/GSAS]]
* [[Combined X-Ray and Neutron Refinements]]
* [[CMPR]]

Latest revision as of 18:48, 22 April 2020

User Wiki for APS Beamline 11-BM

This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.

11-BM News

Archived news and updates about 11-BM and powder diffraction at the APS

Safety & Training

APS Safety & Training Links: https://www.aps.anl.gov/Safety-and-Training/

Experiment Safety Approval Forms (ESAFs): https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page

Experiment Hazard Classes https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions

Sample Preparation

Software

Data Collection/Processing

On-Site Users: Beamline Controls

Data Analysis

Sample Environments

pages for more information on specific environments

Other Equipment

Temperature Controls, Power Supplies etc

Status & History

11-BM Status Page https://11bm.xray.aps.anl.gov/status/status.html

APS Ring Status https://www.aps.anl.gov/Facility/Status/

Video Webcams & Monitors

11-BM Rapid Access

Standards Data

Standards Data: reference powder diffraction data for standard (SRM) samples, plus example fits

Instrument Parameter and Input Files: instrument parameter and input information

11-BM, APS & ANL Links

On-Site Accommodation & Dining

Assorted Links

Software Notes

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