Difference between revisions of "Main Page"

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This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.
== [[11-BM News]] ==
Archived [https://wiki-ext.aps.anl.gov/ug11bm/index.php/11-BM_News news and updates] about 11-BM and powder diffraction at the APS


== Safety & Training ==
== Safety & Training ==
APS Safety & Training Links:
APS Safety & Training Links:
http://www.aps.anl.gov/Safety_and_Training/
https://www.aps.anl.gov/Safety-and-Training/


Experiment Safety Approval Forms (ESAFs):
Experiment Safety Approval Forms (ESAFs):
http://www.aps.anl.gov/Safety_and_Training/Experiment_Safety_Approval_Form/index.html
https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page


Experiment Hazard Classes
Experiment Hazard Classes
http://www.aps.anl.gov/Safety_and_Training/Experiment_Hazard_Classes/index.html
https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions
 
User Policies in APS Central Documents:
http://centraldocs.aps.anl.gov/policy_procedures/user/
 


== Sample Preparation ==
== Sample Preparation ==
* [[Mail-In Powder Diffraction Measurements]]
* [[X-ray Absorption and Fluorescence]]
* [[Samples with Strong X-Ray Absorption]]
* [[Air Sensitive Samples]]
* [[Using Glass or Fused Quartz Capillaries]]
* [[Nesting Glass/Quartz Capillaries in Kapton Tubes]]
* [[Modifying Mail-In Sample Bases]]
* [[On-Site Experiments]]
* [[Supplies and Tools]]
**[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Supplies_and_Tools#Capillaries:_Kapton Capillaries]
* [[Hazards]]
* [[Videos]]


== Software ==


* [http://11bm.xor.aps.anl.gov/documents/11BM_SamplePrepNestedCapillaryKapton.pdf Notes for Sample Prep with Nested Capillaries in Kapton (.pdf download)]
=== Data Collection/Processing ===
 
*[https://11bm.xray.aps.anl.gov/downloads/11BM_SlewScan_Planner.xls 11-BM Slew Scan Parameter Calculator (MS Excel worksheet)]
* Mail-In Sample Prep Notes [http://11bm.xor.aps.anl.gov/users_prep.html @ 11-BM Webpage] or as [http://11bm.xor.aps.anl.gov/documents/11BM_MailInUserInstructions_(BaseShipmentVersion)_Jan2011.pdf .pdf download]
* [https://11bm.xray.aps.anl.gov/absorb/absorb.php ''Absorb'': compute x-ray absorption]
 
* [[Calibration]]
* [[Sample Preparation Gallery]]
* [[Merge]]
 
* [[Off-Site Merge]]
* [[X-ray absorption & fluorescence]]
* Background: see [[Standards Data]]  


 
=== On-Site Users: Beamline Controls===
== Beamline Controls ==
* [[MEDM Status Displays]]
* [[MEDM Status Displays]]
* [[UserControl]]
* [[UserControl]]
* [[new item]]
* [[Sample_Robot]]
 
== Data Collection ==
===Instrument Background===
 
see 11BM webpage for more info:
http://11bm.xor.aps.anl.gov/standards_data.html
 
Plot of background for empty 11-BM 0.8 mm Kapton capillary (@ 30 KeV)
http://11bm.xor.aps.anl.gov/data/standards/Kapton/2010_1/11BM_Kapton.jpg
 
Plot of empty background (no sample or capillary)for 11-BM, air scatter only (@ 30 KeV)
http://11bm.xor.aps.anl.gov/data/standards/background/11BM_background_air_scatter.jpg


=== Data Analysis ===
* [https://11bm.xray.aps.anl.gov/gsasexpgui.html EXPGUI-GSAS] 
* [https://subversion.xray.aps.anl.gov/trac/pyGSAS GSAS-II]
* [https://11bm.xray.aps.anl.gov/cmpr.html CMPR]


== Data Processing ==
== [[Sample Environments]] ==
* [[Calibration]]
* [[Merge]]
* [[Off-Site Merge]]


pages for more information on specific environments


== Equipment ==
* [[Oxford Helium Cryostat]]  
* [[Oxford Helium Cryostat]]
* [[Hot Gas Blower (Cyberstar)]]
* [[Hot Gas Blower (Cyberstar)]]
* [[Gas Handling Equipment]]
* [[Resistive Heating Furnace]]


== Other Equipment ==
Temperature Controls, Power Supplies etc
*[[TEXIO PD18-30AD DC Power Supply]]
*[[SRS PTC10 Temperature Controller]]
*[[KI Flow Meters]]  (for B-hutch Gas Patch Panel)
*[[Goniometer Head Alignment Rig]]


== Status & History ==
== Status & History ==
'''11-BM Status Page'''   
'''11-BM Status Page'''   
http://11bm.xor.aps.anl.gov/status/status.html
https://11bm.xray.aps.anl.gov/status/status.html


APS Ring Status   
APS Ring Status   
http://www.aps.anl.gov/Facility/Status/
https://www.aps.anl.gov/Facility/Status/


* [[11-BM Parameter Log]]
* [[11-BM Parameter Log]]
Line 73: Line 79:
* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]
* [http://twitter.com/#!/APS_11BM/  11BM Twitter Beam Status Feed]


== Video Webcams & Monitors ==
* [https://11bmcam.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted and only viewable onsite)]
* [https://11bmcam2.xray.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted and only viewable onsite)]
* [https://axis.xray.aps.anl.gov/view/index.shtml 11BM Video Server]
* [https://11bm.xray.aps.anl.gov/status/livedata.html 11BM Live Data]
== 11-BM Rapid Access ==
*[[Rapid Access Instructions]]: for mail-in program
*[[Mail-In Bases]]: for mail-in program


== Video Webcams & Monitors ==
== Standards Data ==
* [http://11bmcam.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Side View (restricted)]
[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data Standards Data]:  
* [http://11bmcam2.xor.aps.anl.gov/view/index.shtml 11BM Web Camera:Beam Path View (restricted)]
reference powder diffraction data for standard (SRM) samples, plus example fits
* [http://axis.xor.aps.anl.gov/view/index.shtml 11BM Video Server]
* [http://11bm.xor.aps.anl.gov/status/livedata.html 11BM Live Data]


[https://wiki-ext.aps.anl.gov/ug11bm/index.php/Standards_Data#Instrument_Parameter_and_Input_Files Instrument Parameter and Input Files]:
instrument parameter and input information


== 11-BM, APS & ANL Links ==
== 11-BM, APS & ANL Links ==
11-BM Homepage
*11-BM Homepage: https://11bm.xray.aps.anl.gov/home.html  
http://11bm.xor.aps.anl.gov/home.html  


SRS Group (Sector 11) Homepage
* APS powder diffraction overview sheet [https://11bm.xray.aps.anl.gov/documents/APS_PowderXRD_Flyer_Oct2012.pdf download .pdf]
http://www.aps.anl.gov/Xray_Science_Division/Structural_Science/


APS Beam Status & History
*SRS Group Homepage: https://www.aps.anl.gov/Xray_Science_Division/Structural_Science/
http://www.aps.anl.gov/Facility/Status/


GUP, ESAF & APS Training links
*APS Beam Status & History:  https://www.aps.anl.gov/Facility/Status/
http://www.aps.anl.gov/Users/Current/


APS Beamline Phone Directory
*GUP, ESAF & APS Training links: https://www.aps.anl.gov/Users/Current/
http://www.aps.anl.gov/Beamlines/Phone_Directory/


* [http://www.aps.anl.gov/Users/Contacts/ APS Contacts]
*APS New User Registration: https://www.aps.anl.gov/Users/New/ (see [[User Registration Notes]])
* [http://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]


* [http://www.aim.anl.gov/  Argonne Library (internal only)]
*[[Industrial and Proprietary Users]]


* [http://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
*APS Beamline Phone Directory: https://www.aps.anl.gov/Beamlines/Phone_Directory/
* [http://www.anlgh.org/anlghhome.html Argonne Guest House]


* [[Local Dining Options]]
* [https://www.aps.anl.gov/Users/Contacts/ APS Contacts]
* [https://www.aps.anl.gov/About/Visiting/ ANL Map & visitor links]
* [https://maps.anl.gov/ Interactive Argonne Campus Map]


* [https://www.aim.anl.gov/  Argonne Library (internal only)]
====On-Site Accommodation & Dining====
*[[Off-Site Local Dining Options]]
*[https://www.anlgh.org/Dining/401_Grill/menu.htm 401 Grill]
*[https://www.anlgh.org/anlghhome.html Argonne Guest House]


== Assorted Links ==
== Assorted Links ==
* [[NIST SRM Certificates]]  
* [[NIST SRM Certificates]]  
* [[11BM Calibration Sample: Lattice & Atomic Position Values]]


* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel]
* [http://www.youtube.com/user/s11bm?feature=mhee 11-BM YouTube Video Channel]


* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]
* [http://icsd.fiz-karlsruhe.de/ ICSD Web Access (inorganic crystal structure database, ANL on-site only)]


== GSAS/EXPGUI Notes ==
== Software Notes ==
* [[GSAS Profile Terms]]
* [[Sequential GSAS]]
* [[Sequential GSAS]]
* [[GSAS Refinement Hints]]
* [[GSAS Refinement Hints]]
* [[Preferred orientation in EXPGUI/GSAS]]
* [[Combined X-Ray and Neutron Refinements]]
* [[CMPR]]

Latest revision as of 18:48, 22 April 2020

User Wiki for APS Beamline 11-BM

This wiki contains information for users of the APS beamline 11-BM; new content is added periodically.

11-BM News

Archived news and updates about 11-BM and powder diffraction at the APS

Safety & Training

APS Safety & Training Links: https://www.aps.anl.gov/Safety-and-Training/

Experiment Safety Approval Forms (ESAFs): https://beam.aps.anl.gov/pls/apsweb/esaf0001.start_page

Experiment Hazard Classes https://www.aps.anl.gov/Safety-and-Training/Safety/Using-Material-Samples/Hazardous-Materials/Materials-Hazard-Class-Definitions

Sample Preparation

Software

Data Collection/Processing

On-Site Users: Beamline Controls

Data Analysis

Sample Environments

pages for more information on specific environments

Other Equipment

Temperature Controls, Power Supplies etc

Status & History

11-BM Status Page https://11bm.xray.aps.anl.gov/status/status.html

APS Ring Status https://www.aps.anl.gov/Facility/Status/

Video Webcams & Monitors

11-BM Rapid Access

Standards Data

Standards Data: reference powder diffraction data for standard (SRM) samples, plus example fits

Instrument Parameter and Input Files: instrument parameter and input information

11-BM, APS & ANL Links

On-Site Accommodation & Dining

Assorted Links

Software Notes

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