Difference between revisions of "Resistive Heating Furnace"

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new notes on the Resistive Heating Furnace - under construction Feb 2013


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== Temperature Calibration==
 
See general notes on high temperature calibration here
 
https://wiki-ext.aps.anl.gov/ug11bm/index.php/Hot_Gas_Blower_(Cyberstar)#Temperature_Calibration
 


==Images==
==Images==
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Resistive Heating Furnace - thermocouple, beam and capillary aligned  
Resistive Heating Furnace - thermocouple, beam and capillary aligned  
[[Image:ResistiveHeatingFurnace_A.png|none|400px|ResistiveHeatingFurnace_A.png]]
[[Image:ResistiveHeatingFurnace_A.png|none|400px|ResistiveHeatingFurnace_A.png]]


Resistive Heating Furnace - aligning heater on the capillary  
Resistive Heating Furnace - aligning heater on the capillary  
[[Image:ResistiveHeatingFurnace_B.png|none|400px|ResistiveHeatingFurnace_B.png]]
[[Image:ResistiveHeatingFurnace_B.png|none|400px|ResistiveHeatingFurnace_B.png]]


Resistive Heating Furnace - top view
Resistive Heating Furnace - top view
[[Image:ResistiveHeatingFurnace_C.png|none|400px|ResistiveHeatingFurnace_C.png]]
[[Image:ResistiveHeatingFurnace_C.png|none|400px|ResistiveHeatingFurnace_C.png]]


Resistive Heating Furnace - side view
Resistive Heating Furnace - side view
[[Image:ResistiveHeatingFurnace_D.png|none|400px|ResistiveHeatingFurnace_F.png]]
[[Image:ResistiveHeatingFurnace_D.png|none|400px|ResistiveHeatingFurnace_F.png]]


Resistive Heating Furnace - heat shield removed
Resistive Heating Furnace - heat shield removed
[[Image:ResistiveHeatingFurnace_E.png|none|400px|ResistiveHeatingFurnace_E.png]]
[[Image:ResistiveHeatingFurnace_E.png|none|400px|ResistiveHeatingFurnace_E.png]]


Resistive Heating Furnace - glowing heating elements
Resistive Heating Furnace - glowing heating elements
[[Image:ResistiveHeatingFurnace_F.png|none|400px|ResistiveHeatingFurnace_F.png]]
[[Image:ResistiveHeatingFurnace_F.png|none|400px|ResistiveHeatingFurnace_F.png]]


Controller and [[https://wiki-ext.aps.anl.gov/ug11bm/index.php/TEXIO_PD18-30AD_DC_Power_Supply Power Supply]]
 
[[https://wiki-ext.aps.anl.gov/ug11bm/index.php/SRS_PTC10_Temperature_Controller Controller]] and [[https://wiki-ext.aps.anl.gov/ug11bm/index.php/TEXIO_PD18-30AD_DC_Power_Supply Power Supply]]
[[Image:ResistiveHeatingPowerSupply.png|none|300px|ResistiveHeatingPowerSupply.png]]
[[Image:ResistiveHeatingPowerSupply.png|none|300px|ResistiveHeatingPowerSupply.png]]
== Reference ==
[http://scripts.iucr.org/cgi-bin/paper?S0021889808020165  "A versatile sample-environment cell for non-ambient X-ray scattering experiments."  J Appl Crystallogr (2008) vol. 41 pp. 822-824]

Latest revision as of 18:30, 22 September 2016

Temperature Calibration

See general notes on high temperature calibration here

https://wiki-ext.aps.anl.gov/ug11bm/index.php/Hot_Gas_Blower_(Cyberstar)#Temperature_Calibration


Images

Resistive Heating Furnace - thermocouple, beam and capillary aligned

ResistiveHeatingFurnace_A.png


Resistive Heating Furnace - aligning heater on the capillary

ResistiveHeatingFurnace_B.png


Resistive Heating Furnace - top view

ResistiveHeatingFurnace_C.png


Resistive Heating Furnace - side view

ResistiveHeatingFurnace_F.png


Resistive Heating Furnace - heat shield removed

ResistiveHeatingFurnace_E.png


Resistive Heating Furnace - glowing heating elements

ResistiveHeatingFurnace_F.png


[Controller] and [Power Supply]

ResistiveHeatingPowerSupply.png


Reference

"A versatile sample-environment cell for non-ambient X-ray scattering experiments." J Appl Crystallogr (2008) vol. 41 pp. 822-824