Difference between revisions of "Hot Gas Blower (Cyberstar)"

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== Temperature Calibration ==
== Temperature Calibration ==
=== Al2O3 & Pt Thermal Expansion ===   
=== Al2O3 & Pt Thermal Expansion ===   
J. Appl. Cryst. (1993). 26, 77-81    [ doi:10.1107/S002188989200877X ]
"High-temperature X-ray diffraction: solutions to uncertainties in temperature and sample position"
N. E. Brown, S. M. Swapp, C. L. Bennett and A. Navrotsky


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Revision as of 18:34, 24 September 2012

About

11-BM has a dedicated Cyberstar Hot Gas Blower. This can be used to heat small diameter capillary samples from ambient temperature to ~ 950 °C

About

Temperature Range and Ramp Rate.

  • ambient temperature to ~ 950 °C
  • Max ramp rate on heating & cooling is 5 deg C/min (300 C/hour)

Users should plan experiments to incorporate these heating and cooling ramp times.


11-BM Hot Gas Blower Image

Hot Air Blower Zoomed Image


Temperature Profile & Alignment

GasBlowerProfile

Temperature Calibration

Al2O3 & Pt Thermal Expansion

J. Appl. Cryst. (1993). 26, 77-81 [ doi:10.1107/S002188989200877X ] "High-temperature X-ray diffraction: solutions to uncertainties in temperature and sample position" N. E. Brown, S. M. Swapp, C. L. Bennett and A. Navrotsky


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Phase Transitions

HotGasBlowerTempCalib.png

SiO2

HotGasBlowerSiO2Heating HotGasBlowerSiO2Cooling

PbTiO3

HotGasBlowerPbTiO3