Difference between revisions of "11BM Calibration Sample: Lattice & Atomic Position Values"
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Calibration of the wavelength at 11-BM is performed using a mixture of NIST standard reference materials (SRMs). | Calibration of the wavelength at 11-BM is performed using a mixture of NIST standard reference materials (SRMs). | ||
As of 2011, the calibration sample is a mixture of ~ 70 wt% Si (SRM | As of 2011, the calibration sample is a mixture of ~ 70 wt% Si (SRM 640d) and ~ 30 wt% Al2O3 (SRM 676). | ||
Lattice & Atomic Position Values are as follows: | Lattice & Atomic Position Values are as follows: | ||
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Si (SRM 640d) | Si (SRM 640d) | ||
Space Group: F d -3 m | Space Group: F d -3 m | ||
Lattice: 5. | Lattice: 5.431590 5.431590 5.431590 90.0000 90.0000 90.0000 | ||
Atom1: Si @ x = 1/8, y = 1/8, z = 1/8 | Atom1: Si @ x = 1/8, y = 1/8, z = 1/8 | ||
| Line 16: | Line 16: | ||
Atom1: Al @ x = 0, y = 0, z = 0.351869 | Atom1: Al @ x = 0, y = 0, z = 0.351869 | ||
Atom2: O @ x = 0.307804, y = 0, z = 1/4 | Atom2: O @ x = 0.307804, y = 0, z = 1/4 | ||
As of 13 February 2013, we started using the revised certification for 640d, | |||
for which the parameters are | |||
Si (SRM 640d) | |||
Space Group: F d -3 m | |||
Lattice: 5.431230 5.431230 5.431230 90.0000 90.0000 90.0000 | |||
Atom1: Si @ x = 1/8, y = 1/8, z = 1/8 | |||
Latest revision as of 22:46, 14 February 2013
Calibration of the wavelength at 11-BM is performed using a mixture of NIST standard reference materials (SRMs).
As of 2011, the calibration sample is a mixture of ~ 70 wt% Si (SRM 640d) and ~ 30 wt% Al2O3 (SRM 676).
Lattice & Atomic Position Values are as follows:
Si (SRM 640d) Space Group: F d -3 m Lattice: 5.431590 5.431590 5.431590 90.0000 90.0000 90.0000 Atom1: Si @ x = 1/8, y = 1/8, z = 1/8
Al2O3 (SRM 676a) Space Group: R -3 c Lattice: 4.7590914 4.7590914 12.991779 90.0000 90.0000 120.0000 Atom1: Al @ x = 0, y = 0, z = 0.351869 Atom2: O @ x = 0.307804, y = 0, z = 1/4
As of 13 February 2013, we started using the revised certification for 640d, for which the parameters are
Si (SRM 640d) Space Group: F d -3 m Lattice: 5.431230 5.431230 5.431230 90.0000 90.0000 90.0000 Atom1: Si @ x = 1/8, y = 1/8, z = 1/8
