Rapid Access Instructions - Revision history

WikiSysop: /* SHIPPING: */

2014-10-03T19:29:54Z

SHIPPING:

← Older revision		Revision as of 19:29, 3 October 2014
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	'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples		'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples

	[[Image:brokenglasssamples.~~png~~\|300px\|File:brokenglasssamples.~~png~~]]		[[Image:brokenglasssamples.jpg\|300px\|File:brokenglasssamples.jpg]]

	Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.		Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.

WikiSysop: /* SHIPPING: */

2014-10-03T19:29:04Z

SHIPPING:

← Older revision		Revision as of 19:29, 3 October 2014
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	'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples		'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples

	[[Image:brokenglasssamples.~~jpg~~\|300px\|File:brokenglasssamples.~~jpg~~]]		[[Image:brokenglasssamples.png\|300px\|File:brokenglasssamples.png]]

	Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.		Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.

WikiSysop at 19:28, 3 October 2014

2014-10-03T19:28:06Z

← Older revision		Revision as of 19:28, 3 October 2014
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	Rapid Access Instructions can be downloaded as a [[~~https~~://~~subversion~~.~~xor~~.aps.anl.gov~~/11BMweb/External/trunk~~/documents/~~11BM_MailInUserInstructions_Oct2012~~.pdf .pdf file]].		Rapid Access Instructions can be downloaded as a [[http://11bm.xray.aps.anl.gov/documents/11BM_MailInUserInstructions_Feb2013.pdf .pdf file]].


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	'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples		'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples

	[[File:brokenglasssamples.jpg]]		[[Image:brokenglasssamples.jpg\|300px\|File:brokenglasssamples.jpg]]

	Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.		Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.
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	[[Image:sampleprep.png\|800px\|sampleprep.png]]		[[Image:sampleprep.png\|800px\|sampleprep.png]]


	==OBTAINING DATA:==		==OBTAINING DATA:==

WikiSysop: /* SHIPPING: */

2014-10-03T19:26:14Z

SHIPPING:

← Older revision		Revision as of 19:26, 3 October 2014
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	==SHIPPING:==		==SHIPPING:==
	Users are responsible for shipping samples to Argonne in full compliance with DOT rules and regulations (see Safety Notice above). You may use the US Mail or a commercial shipping company (FedEx, UPS, DHL, etc). We recommend protecting samples in bubble wrap (provided) or some other padding during shipment. Do not add a signature requirement for delivery of your package.		Users are responsible for shipping samples to Argonne in full compliance with DOT rules and regulations (see Safety Notice above). You may use the US Mail or a commercial shipping company (FedEx, UPS, DHL, etc). We recommend protecting samples in bubble wrap (provided) or some other padding during shipment. Do not add a signature requirement for delivery of your package.

			'''GLASS Regulation''': The use of glass vials, ampoules or other containers for shipping 11-BM samples to the APS is now prohibited. (excluding nested sample quartz capillaries). Instead, simply use bubble wrap or plastic containers. Most of the time, glass containers are broken on arrival at the APS, which is dangerous for beamline staff and does nothing to protect your samples

			[[File:brokenglasssamples.jpg]]

	Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.		Email notification is sent when samples are received. We are unable track shipped samples or sample base kits.

WikiSysop at 17:06, 9 October 2012

2012-10-09T17:06:48Z

← Older revision		Revision as of 17:06, 9 October 2012
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	~~wiki page under construction,~~

	~~see http://11bm.xray.aps.anl.gov/instructions.html~~

	~~----~~

	Rapid Access Instructions can be downloaded as a [[https://subversion.xor.aps.anl.gov/11BMweb/External/trunk/documents/11BM_MailInUserInstructions_Oct2012.pdf .pdf file]].		Rapid Access Instructions can be downloaded as a [[https://subversion.xor.aps.anl.gov/11BMweb/External/trunk/documents/11BM_MailInUserInstructions_Oct2012.pdf .pdf file]].

WikiSysop: /* SAMPLE BASE KIT: */

2012-10-09T17:06:22Z

SAMPLE BASE KIT:

← Older revision		Revision as of 17:06, 9 October 2012
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	*Kapton Capillary Tubes: to contain samples. The inner diameter of the supplied tube is 0.80 mm. The outside diameter fits snugly inside the mounting base. '''All samples (powders, foils, nested capillaries, etc.) must be fully contained and secured within straight Kapton tubes.''' Samples are spun at high speed during data collection. Non-secured samples will shift or move out of the beam position when spun. We cannot mount unsecured or bend samples. Kapton tubes are provided for your convenience. Kapton is stable over a wide temperature range and adds a negligible contribution to the diffraction scan background.		*Kapton Capillary Tubes: to contain samples. The inner diameter of the supplied tube is 0.80 mm. The outside diameter fits snugly inside the mounting base. '''All samples (powders, foils, nested capillaries, etc.) must be fully contained and secured within straight Kapton tubes.''' Samples are spun at high speed during data collection. Non-secured samples will shift or move out of the beam position when spun. We cannot mount unsecured or bend samples. Kapton tubes are provided for your convenience. Kapton is stable over a wide temperature range and adds a negligible contribution to the diffraction scan background.

	[[Image:mailinkit.png\|~~250px~~\|mailinkit.png]]		[[Image:mailinkit.png\|300px\|mailinkit.png]]


	==PROHIBITED SAMPLE HAZARDS:==		==PROHIBITED SAMPLE HAZARDS:==

WikiSysop: /* SAMPLE PREPARATION: */

2012-10-09T17:06:13Z

SAMPLE PREPARATION:

← Older revision		Revision as of 17:06, 9 October 2012
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	Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.		Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.

	[[Image:sampleprep.png\|~~500px~~\|sampleprep.png]]		[[Image:sampleprep.png\|800px\|sampleprep.png]]

	==OBTAINING DATA:==		==OBTAINING DATA:==

WikiSysop: /* SAMPLE PREPARATION: */

2012-10-09T17:05:58Z

SAMPLE PREPARATION:

← Older revision		Revision as of 17:05, 9 October 2012
Line 98:		Line 98:
	Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.		Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.

	[[Image:sampleprep.png\|~~400px~~\|sampleprep.png]]		[[Image:sampleprep.png\|500px\|sampleprep.png]]

	==OBTAINING DATA:==		==OBTAINING DATA:==

WikiSysop: /* SAMPLE PREPARATION: */

2012-10-09T17:05:46Z

SAMPLE PREPARATION:

← Older revision		Revision as of 17:05, 9 October 2012
Line 98:		Line 98:
	Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.		Figures below illustrate a properly prepared sample for the 11-BM mail-in service, including the position of the X-ray beam on the sample capillary tube. Red material visible at the capillary tip is modeling clay used to secure powder inside the Kapton tube. See the 11-BM webpage for larger images and advice on sample preparation.

	[[Image:sampleprep.png\|~~250px~~\|sampleprep.png]]		[[Image:sampleprep.png\|400px\|sampleprep.png]]


	==OBTAINING DATA:==		==OBTAINING DATA:==

WikiSysop: /* REGISTRATION & SCAN REQUESTS: */

2012-10-09T17:05:35Z

REGISTRATION & SCAN REQUESTS:

← Older revision		Revision as of 17:05, 9 October 2012
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	Select scan parameters for each sample using the pull-down menus. Select a standard (≈ 1 hour) scan at room temperature '''Ambient''' or low temperature '''100 K.''' Alternatively, select '''Other''' from the menu to request non-standard scan types or temperatures (100 - 450 K), or to select multiple scans (i.e. two temperatures) for a single sample. Note custom scan requests are added on a subsequent webpage (this page appears only after clicking on the "Register Sample Info" button to proceed). See 11-BM webpages for custom scan options & restrictions.		Select scan parameters for each sample using the pull-down menus. Select a standard (≈ 1 hour) scan at room temperature '''Ambient''' or low temperature '''100 K.''' Alternatively, select '''Other''' from the menu to request non-standard scan types or temperatures (100 - 450 K), or to select multiple scans (i.e. two temperatures) for a single sample. Note custom scan requests are added on a subsequent webpage (this page appears only after clicking on the "Register Sample Info" button to proceed). See 11-BM webpages for custom scan options & restrictions.

	[[Image:scanrequest.png\|~~50px~~\|scanrequest.png]]		[[Image:scanrequest.png\|100px\|scanrequest.png]]

	When prompted by email, you must take action to confirm the registration information. This “e-signature” is necessary to comply with APS and DOE safety regulations.		When prompted by email, you must take action to confirm the registration information. This “e-signature” is necessary to comply with APS and DOE safety regulations.