Difference between revisions of "34-ID-C"

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A small liquid flow cell is available with a peristaltic pump.  A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam.  The same cell is often used for room temperature gas flow experiments.
A small liquid flow cell is available with a peristaltic pump.  A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam.  The same cell is often used for room temperature gas flow experiments.


 
[[File:liquidcell1.jpg]]


'''Coin Cell holder'''
'''Coin Cell holder'''

Revision as of 20:02, 24 February 2018

Setup Images and Drawings

Media: 34IDC_basic_instrument_diagrams_for_mounting_assistance_etc.pdf

Sample Environments (Resident at beamline)

Heater Cell

The heater cell is capable of several hundred degrees centigrade. Improvements are underway to reach up to 1000 C. It also supports a single gas flow through the chamber. It is not vacuum compatible.

Heater1.jpg Heater2.jpg


Linkam Cryo stage

The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber, than that pictured, includes a magnetically secured removable cover.

Linkam1.JPG Linkam2.jpg

Liquid/Gas Flow Cell

A small liquid flow cell is available with a peristaltic pump. A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam. The same cell is often used for room temperature gas flow experiments.

Liquidcell1.jpg

Coin Cell holder

In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.

Coincell1.jpg Coincell2.jpg Echemlab.png

Available Detectors

add stuff here

Publications

Our full publication list