Difference between revisions of "34-ID-C"

From 34-ID-C
Jump to navigationJump to search
Line 28: Line 28:
In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.
In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.


[[File:coincell1.jpg|320px]]  [[File:coincell2.jpg|320px]]  [[File:echemlab.jpg|240px]]
[[File:coincell1.jpg|320px]]  [[File:coincell2.jpg|320px]]  [[File:Echemlab.png|240px]]


== Available Detectors ==
== Available Detectors ==

Revision as of 19:58, 24 February 2018

Setup Images and Drawings

Media: 34IDC_basic_instrument_diagrams_for_mounting_assistance_etc.pdf

Sample Environments (Resident at beamline)

Heater Cell

The heater cell is capable of several hundred degrees centigrade. Improvements are underway to reach up to 1000 C. It also supports a single gas flow through the chamber. It is not vacuum compatible.

Heater1.jpg Heater2.jpg


Linkam Cryo stage

The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber, than that pictured, includes a magnetically secured removable cover.

Linkam1.JPG Linkam2.jpg

Liquid/Gas Flow Cell

A small liquid flow cell is available with a peristaltic pump. A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam. The same cell is often used for room temperature gas flow experiments.


Coin Cell holder

In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.

Coincell1.jpg Coincell2.jpg Echemlab.png

Available Detectors

add stuff here

Publications

Our full publication list