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<bibtex>
== Apply for beamtime at 34-ID-C ==
@article{Ulvestad:2014gj,
author = {Ulvestad, A and Cho, H M and Harder, R and Kim, J W and Dietze, S H and Fohtung, E and Meng, Y S and Shpyrko, O G},
title = {{Nanoscale strain mapping in battery nanostructures}},
journal = {Applied Physics Letters},
year = {2014},
volume = {104},
number = {7},
pages = {073108},
month = feb
}
</bibtex>
<bibtex>
@article{Dufresne:2012p17466,
author = {Dufresne, Eric M and Adams, Bernhard and Chollet, Matthieu and Harder, Ross and Li, Yuelin and Wen, Haidan and Leake, Steven J and Beitra, Loren and Huang, Xiaojing and Robinson, Ian K},
title = {{A technique for high-frequency laser-pump X-ray probe experiments at the APS}},
journal = {Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment},
year = {2011},
volume = {649},
number = {1},
pages = {191--193},
month = jan
}
</bibtex>
@article{Newton:2010p17906,
author = {Newton, Marcus C and Leake, Steven J and Harder, Ross and Robinson, Ian K},
title = {{Three-dimensional imaging of strain in a single ZnO nanorod}},
journal = {Nat Mater},
year = {2009},
volume = {9},
number = {2},
pages = {120--124},
month = dec,
annote = {10.1038/nmat2607}
}
@inproceedings{Cha:2009p18938,
author = {Cha, Wonsuk and Song, Sanghoon and Jeong, Nak Cheon and Yoon, Kyung Byung and Harder, Ross and Robinson, Ian K and Kim, Hyunjung and Hartline, Beverly Karplus and Horton, Renee K and Kaicher, Catherine M},
title = {{Coherent X-ray Diffraction Imaging of Zeolite Microcrystals (abstract)}},
booktitle = {WOMEN IN PHYSICS: Third IUPAP International Conference on Women in Physics},
year = {2009},
pages = {207--207},
publisher = {AIP}
}
@article{Harder:2011p18939,
author = {Harder, Ross and Xiao, X},
title = {{Coherent Cone-Beam X-ray Microscopy}},
journal = {AIP Conference Proceedings},
year = {2011},
volume = {1365},
number = {1},
pages = {429--432}
}
@article{Shi:2013vs,
author = {Shi, Xiaowen},
title = {{Coherent X-ray diffraction imaging and ptychography on silicon-on-insulator nanostructures}},
year = {2013},
pages = {1--243},
month = mar
}
@article{Xiong:2011p18792,
author = {Xiong, Gang and Moutanabbir, Oussama and Huang, Xiaojing and Paknejad, Seyed A and Shi, Xiaowen and Harder, Ross and Reiche, Manfred and Robinson, Ian K},
title = {{Elastic relaxation in an ultrathin strained silicon-on-insulator structure}},
journal = {Applied Physics Letters},
year = {2011},
volume = {99},
number = {11},
pages = {114103}
}
@article{Newton:2010p5204,
author = {Newton, Marcus and Harder, Ross and Huang, Xiaojing and Xiong, Gang and Robinson, Ian},
title = {{Phase retrieval of diffraction from highly strained crystals}},
journal = {Physical Review B},
year = {2010},
volume = {82},
number = {16},
pages = {165436}
}
@article{StevenJLeake:2011p20967,
author = {Leake, Steven J and Harder, Ross and Robinson, Ian K},
title = {{Coherent diffractive imaging of solid state reactions in zinc oxide crystals}},
journal = {New Journal of Physics},
year = {2011},
volume = {13},
number = {11},
pages = {113009},
month = nov
}
@article{Holt:2013fha,
author = {Holt, Martin and Harder, Ross and Winarski, Robert and Rose, Volker},
title = {{Nanoscale Hard X-Ray Microscopy Methods for Materials Studies*}},
journal = {Annu. Rev. Mater. Res.},
year = {2013},
volume = {43},
number = {1},
pages = {183--211},
month = jan
}
@article{Huang:2012p22325,
author = {Huang, Xiaojing and Wojcik, Michael and Burdet, Nicolas and Peterson, Isaac and Morrison, Graeme and Vine, David J and Legnini, Daniel and Harder, Ross and Chu, Yong S and Robinson, Ian},
title = {{Quantitative X-ray wavefront measurements of Fresnel zone plate and K-B mirrors using phase retrieval}},
journal = {Opt. Express},
year = {2012},
volume = {20},
number = {21},
pages = {24038--24048}
}
@article{Poynor:2006cp,
author = {Poynor, Adel{\'e} and Hong, Liang and Robinson, Ian and Granick, Steve and Zhang, Zhan and Fenter, Paul},
title = {{How Water Meets a Hydrophobic Surface}},
journal = {Physical review letters},
year = {2006},
volume = {97},
number = {26},
pages = {266101},
month = dec
}
@article{Vartanyants:2007do,
author = {Vartanyants, I A and Robinson, I K and McNulty, I and David, C and Wochner, P and Tschentscher, Th},
title = {{Coherent X-ray scattering and lensless imaging at the European XFEL Facility}},
journal = {Journal of Synchrotron Radiation},
year = {2007},
volume = {14},
number = {6},
pages = {453--470},
month = nov
}
@article{Cha:2010p153,
author = {Cha, Wonsuk and Song, Sanghoon and Jeong, Nak Cheon and Harder, Ross and Yoon, Kyung Byung and Robinson, Ian K and Kim, Hyunjung},
title = {{Exploration of crystal strains using coherent x-ray diffraction}},
journal = {New Journal of Physics},
year = {2010},
volume = {12},
number = {3},
pages = {035022},
month = mar
}
@article{Harder:2007p17865,
author = {Harder, R and Pfeifer, M and williams, G and Vartaniants, I and Robinson, I},
title = {{Orientation variation of surface strain}},
journal = {Physical Review B},
year = {2007},
volume = {76},
number = {11},
pages = {115425},
month = sep
}
@article{1367-2630-13-3-033006,
author = {Xiong, Gang and Huang, Xiaojing and Leake, Steven J and Newton, Marcus C and Harder, Ross and Robinson, Ian K},
title = {{Coherent x-ray diffraction imaging of ZnO nanostructures under confined illumination}},
journal = {New Journal of Physics},
year = {2011},
volume = {13},
number = {3},
pages = {033006},
month = mar
}
@article{Shi:2012hm,
author = {Shi, Xiaowen and Xiong, Gang and Huang, Xiaojing and Harder, Ross and Robinson, Ian},
title = {{Radiation-induced bending of silicon-on-insulator nanowires probed by coherent x-ray diffractive imaging}},
journal = {New Journal of Physics},
year = {2012},
volume = {14},
number = {6},
pages = {063029},
month = jun
}
@article{1367-2630-12-3-035019,
author = {Harder, Ross and Liang, M and Sun, Y and Xia, Y and Robinson, I K},
title = {{Imaging of complex density in silver nanocubes by coherent x-ray diffraction}},
journal = {New Journal of Physics},
year = {2010},
volume = {12},
number = {3},
pages = {035019},
month = mar
}
@article{ChenDr:2011p19101,
author = {Chen, Yu-chen Karen},
title = {{ykchen_thesis_20110913_final}},
year = {2011}
}
@article{Cha:2013fxa,
author = {Cha, Wonsuk and Jeong, Nak Cheon and Song, Sanghoon and Park, Hyun-jun and Pham, Tung Cao Thanh and Harder, Ross and Lim, Bobae and Xiong, Gang and Ahn, Docheon and McNulty, Ian and Kim, Jungho and Yoon, Kyung Byung and Robinson, Ian K and Kim, Hyunjung},
title = {{Core--shell strain structure of zeolite microcrystals}},
journal = {Nat Mater},
year = {2013},
volume = {12},
number = {8},
pages = {729--734},
month = jul
}
@article{Watari:2011p19116,
author = {Watari, Moyu and McKendry, Rachel A and V{\"o}gtli, Manuel and Aeppli, Gabriel and Soh, Yeong-Ah and Shi, Xiaowen and Xiong, Gang and Huang, Xiaojing and Harder, Ross and Robinson, Ian K},
title = {{Differential stress induced by thiol adsorption on facetted nanocrystals}},
journal = {Nat Mater},
year = {2011},
volume = {10},
number = {11},
pages = {862--866},
month = sep,
annote = {10.1038/nmat3124}
}


@inproceedings{2004AIPC..705..651K,
[https://www.aps.anl.gov/Users-Information APS Users Information]
author = {Kupp, Tom and Blank, Basil and Deyhim, Alex and Benson, Curtis and Robinson, Ian and Fuoss, Paul},
title = {{Development of a Double Crystal Monochromator}},
booktitle = {SYNCHROTRON RADIATION INSTRUMENTATION: Eighth International Conference on Synchrotron Radiation Instrumentation. AIP Conference Proceedings},
year = {2004},
pages = {651--654},
organization = {Advanced Design Consulting, Inc adcatadc9001.com},
month = may
}


@article{Robinson:2000p17468,
== Publications ==
author = {Benson, Curtis and Robinson, Ian},
title = {{Beam splitting mirror for advanced photon source sector 34}},
journal = {AIP Conference Proceedings},
year = {2000},
volume = {521},
number = {1},
pages = {230--233},
month = jan
}


@article{Badger:2013fd,
[https://www.aps.anl.gov/Sectors-33-34/Publications/34-ID-C '''Our current publication list''']
author = {Badger, John and Lal, Jyotsana and Harder, Ross and Inouye, Hideyo and Gleber, S Charlotte and Vogt, Stefan and Robinson, Ian and Makowski, Lee},
title = {{Three-dimensional Imaging of Crystalline Inclusions Embedded in Intact Maize Stalks.}},
journal = {Scientific reports},
year = {2013},
volume = {3},
pages = {2843},
month = oct
}


@article{Robinson:2009p17908,
== Setup Images and Drawings ==
author = {Robinson, Ian and Harder, Ross},
title = {{Coherent X-ray diffraction imaging of strain at the nanoscale}},
journal = {Nat Mater},
year = {2009},
volume = {8},
number = {4},
pages = {291--298},
month = apr,
annote = {10.1038/nmat2400}
}


@article{Liang:2005jm,
[[Media: 34IDC_basic_instrument_diagrams_2022.pdf]]
author = {Liang, Hongjun and Harries, Daniel and Wong, Gerard C L},
title = {{Polymorphism of DNA--anionic liposome complexes reveals hierarchy of ion-mediated interactions}},
journal = {Proceedings of the National Academy of Sciences of the United States of America},
year = {2005},
volume = {102},
number = {32},
pages = {11173--11178},
month = jan
}


@article{Robinson:2005p9498,
Specs:
author = {Robinson, I K and Da, Y and Spila, T and Greene, J E},
title = {{Coherent diffraction patterns of individual dislocation strain fields}},
journal = {Journal of Physics D: Applied Physics},
year = {2005},
volume = {38},
number = {10A},
pages = {A7--A10},
month = may
}


@article{Boutet:2005ec,
The detector arm can move in two dimensions.
author = {Boutet, S{\'e}bastien and Robinson, Ian K},
title = {{Radiation driven collapse of protein crystals}},
journal = {Journal of Synchrotron Radiation},
year = {2005},
volume = {13},
number = {1},
pages = {1--7},
month = dec
}


@article{Sadleir:2006jf,
Delta: -2 -> 45 degrees
author = {Sadleir, J E and Bandler, S R and Brekosky, R P and Chervenak, J and Figueroa-Feliciano, E and Finkbeiner, F and Iyomoto, N and Kelley, R L and Kilbourne, C A and King, J M and Porter, F S and Robinson, I K and Saab, T and Talley, D J},
title = {{Bismuth X-ray absorber studies for TES microcalorimeters}},
journal = {Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment},
year = {2006},
volume = {559},
number = {2},
pages = {447--449},
month = apr
}


@article{Pfeifer:2006p14842,
Gamma: -2 -> 150 degrees
author = {Pfeifer, Mark A and Williams, Garth J and Vartanyants, Ivan A and Harder, Ross and Robinson, Ian K},
title = {{Three-dimensional mapping of a deformation field inside a nanocrystal}},
journal = {Nature},
year = {2006},
volume = {442},
number = {7098},
pages = {63--66},
month = jul,
annote = {10.1038/nature04867}
}


@article{2003OExpr..11.2329R,
Delta is the axis perpendicular to the floor, essentially moves the detector horizontally.
author = {Robinson, Ian and Pfeiffer, Franz and Vartanyants, Ivan and Sun, Yugang and Xia, Younan},
The range of Delta is -2 to 45 degrees. Although it can be a little larger if the other detector axis is increased.
title = {{Enhancement of coherent X-ray diffraction from nanocrystals by introduction of X-ray optics}},
Gamma is the axis parallel to the floor.  It effectively moves the detector up and down.  The range is dependent on the configuration of the instrument.  It can be as much as 150 degrees.
journal = {Opt. Express},
year = {2003},
volume = {11},
number = {19},
pages = {2329--2334},
month = jan
}


@article{Vartanyants:2003kw,
== Sample Environments (Resident at beamline) ==
author = {Vartanyants, I A and Robinson, I K},
title = {{Imaging of quantum array structures with coherent and partially coherent diffraction}},
journal = {Journal of Synchrotron Radiation},
year = {2003},
volume = {10},
number = {6},
pages = {409--415},
month = nov
}


@article{Pfeiffer:2004bv,
'''Current Gas Inventory '''
author = {Pfeiffer, Franz and Zhang, Wei and Robinson, Ian K},
title = {{Coherent grazing exit x-ray scattering geometry for probing the structure of thin films}},
journal = {Applied Physics Letters},
year = {2004},
volume = {84},
number = {11},
pages = {1847}
}


@inproceedings{Rau:2004ev,
Updated every few weeks.
author = {Rau, Christoph and Peterson, K M and Jemian, P R and Terry, T and Harris, Michael T and Vogt, Stefan and Richter, C P and Neuhausler, U and Schneider, G and Robinson, Ian K},
[https://docs.google.com/spreadsheets/d/1yFvu0P6Ck9RPwrFgc0DReVKp1bYSi-gFenb9BOYoTDw/edit?usp=sharing '''34-ID-C gases in stock''']
title = {{The evolution of hard x-ray tomography from the micrometer to the nanometer length scale}},
booktitle = {Optical Science and Technology, the SPIE 49th Annual Meeting},
year = {2004},
editor = {Bonse, Ulrich},
pages = {709--714},
publisher = {SPIE},
month = oct
}


@article{Yang:2004bz,
'''Kinematic Sample Mount'''
author = {Yang, Lihua and Liang, Hongjun and Angelini, Thomas E and Butler, John and Coridan, Robert and Tang, Jay X and Wong, Gerard C L},
title = {{Self-assembled virus--membrane complexes}},
journal = {Nat Mater},
year = {2004},
volume = {3},
number = {9},
pages = {615--619},
month = aug
}


@inproceedings{Rau:2006eq,
The typical sample mount for STP measurements in air is a Thorlabs KBT1x1 magnetic kinematic mount.  The usual fixation method is double sided sticky tape, though wax and nail polish are available.
author = {Rau, C and Crecea, V and Richter, C P and Peterson, K M and Jemian, P R and Neuhausler, U and Schneider, G and Yu, X and Braun, P V and Chiang, T C and Robinson, I K},
title = {{A hard x-ray KB-FZP microscope for tomography with sub-100-nm resolution}},
booktitle = {Optics {\&} Photonics},
year = {2006},
editor = {Bonse, Ulrich},
pages = {63181G--63181G--6},
publisher = {SPIE},
month = aug
}


@article{Rau:2006hu,
[[File:kinematicsamplemount.jpg|320px]]
author = {Rau, C and Robinson, I K and Richter, C P},
title = {{Visualizing soft tissue in the mammalian cochlea with coherent hard X-rays}},
journal = {Microscopy Research and Technique},
year = {2006},
volume = {69},
number = {8},
pages = {660--665}
}


@article{Li:2006gd,
author = {Li, B and Brody, H D and Black, D R and Burdette, H E and Rau, C},
title = {{Real time observation of dendritic solidification in alloys by synchrotron microradiography}},
journal = {Journal of Physics D: Applied Physics},
year = {2006},
volume = {39},
number = {20},
pages = {4450--4456},
month = sep
}


@article{Li:2006jy,
'''Heater Cell'''
author = {Li, B and Brody, H D and Black, D R and Burdette, H E and Rau, C},
title = {{A compact design of a temperature gradient furnace for synchrotron microradiography}},
journal = {Measurement Science and Technology},
year = {2006},
volume = {17},
number = {7},
pages = {1883--1887},
month = jun
}


@article{Leake:2009p17903,
The heater cell is capable of several hundred degrees centigrade.  Improvements are underway to reach up to 1000 C.  It also supports gas flow through the chamber.  It is not vacuum compatible.
author = {Leake, Steven J and Newton, Marcus and Harder, Ross and Robinson, Ian},
title = {{Longitudinal coherence function in X-ray imaging of crystals}},
journal = {Opt. Express},
year = {2009},
volume = {17},
number = {18},
pages = {15853--15859}
}


@article{Huang:2011p17902,
[[File:Heater1.jpg|320px]] [[File:Heater2.jpg|320px]]
author = {Huang, Xiaojing and Harder, Ross and Xiong, Gang and Shi, Xiaowen and Robinson, Ian},
title = {{Propagation uniqueness in three-dimensional coherent diffractive imaging}},
journal = {Physical Review B},
year = {2011},
volume = {83},
number = {22},
pages = {224109}
}


@article{Rau:2007wz,
author = {Rau, C and Crecea, V and Peterson, K M and Jemian, P R and Richter, C P and Neuhausler, U and Schmeider, G and Yu, X and Braun, P V and Robinson, I K UIUC and {NWU} and {Bessy} and {U Bielefeld}},
title = {{A Full-Field KB-FZP Microscope for Hard X-Ray Imaging with Sub 100 nm Resolution}},
journal = {Conference: Proceedings of the 8th International Conference on X-ray Microscopy;26-30 July 2005},
year = {2007},
month = jun
}


@article{Zribi:2006dx,
author = {Zribi, Olena and Kyung, Hee and Golestanian, Ramin and Liverpool, Tanniemola and Wong, Gerard},
title = {{Condensation of DNA-actin polyelectrolyte mixtures driven by ions of different valences}},
journal = {Physical Review E},
year = {2006},
volume = {73},
number = {3},
pages = {031911},
month = mar
}


@article{Williams:2006cb,
author = {Williams, Garth and Pfeifer, Mark and Vartanyants, Ivan and Robinson, Ian},
title = {{Effectiveness of iterative algorithms in recovering phase in the presence of noise}},
journal = {Acta Crystallographica Section A Foundations of Crystallography},
year = {2006},
volume = {63},
number = {1},
pages = {36--42},
month = dec
}


@article{Solomonov:2007dv,
'''Linkam Cryo stage'''
author = {Solomonov, Inna and Osipova, Maria and Feldman, Yishay and Baehtz, Carsten and Kjaer, Kristian and Robinson, Ian K and Webster, Grant T and McNaughton, Don and Wood, Bayden R and Weissbuch, Isabelle and Leiserowitz, Leslie},
title = {{Crystal Nucleation, Growth, and Morphology of the Synthetic Malaria Pigment $\beta$-Hematin and the Effect Thereon by Quinoline Additives:  The Malaria Pigment as a Target of Various Antimalarial Drugs}},
journal = {Journal Of The American Chemical Society},
year = {2007},
volume = {129},
number = {9},
pages = {2615--2627},
month = mar
}


@article{Rau:2007cq,
The guts of this cell is a Linkam THMS controller.  Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant.  Development of a highly dried gas environment is underway to minimize icing.  The cell can also support moderate heating, limited by melting the 3D printed chamber.  We have maintained 50 C for many hours with no problem. A newer version of the chamber includes a magnetically secured removable cover.
author = {Rau, C and Crecea, V and Richter, C P and Peterson, K M and Jemian, P R and Neuhausler, U and Schneider, G and Yu, X and Braun, P V and Chiang, T C and Robinson, I K},
title = {{braungroup.beckman.illinois.edu/reprints/reprintscopy/pvb061.pdf}},
journal = {Micro {\&} Nano Letters},
year = {2007},
volume = {2},
number = {1},
pages = {1}
}


@article{Rau:2007jv,
[[File:Linkam1.JPG|320px]]  [[File:Linkam2.jpg|240px]]
author = {Rau, C and Crecea, V and Liu, W and Richter, C P and Peterson, K M and Jemian, P R and Neuhausler, U and Schneider, G and Yu, X and Braun, P V and Chiang, T C and Robinson, I K},
title = {{Synchrotron-based imaging and tomography with hard X-rays}},
journal = {Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms},
year = {2007},
volume = {261},
number = {1-2},
pages = {850--854},
month = aug
}


@article{Felici:2007ig,
author = {Felici, R and Jeutter, N M and Mussi, V and de Mongeot, F Buatier and Boragno, C and Valbusa, U and Toma, A and Zhang, Y Wei and Rau, C and Robinson, I K},
title = {{In situ study of the dewetting behavior of Ni-films on oxidized Si(001) by GISAXS}},
journal = {Surface science},
year = {2007},
volume = {601},
number = {18},
pages = {4526--4530},
month = sep
}


@article{Zhang:2007fu,
author = {Zhang, Wei and Robinson, Ian K},
title = {{Grazing exit small angle X-ray scattering on grain formation in polycrystalline metal films}},
journal = {Zeitschrift f{\"u}r Kristallographie},
year = {2007},
volume = {222},
number = {11/2007},
pages = {601},
month = aug
}


@article{Boutet:2007gs,
author = {Boutet, S and Robinson, I},
title = {{Precrystallization clusters of holoferritin and apoferritin at low temperature}},
journal = {Physical Review E},
year = {2007},
volume = {75},
number = {2},
pages = {021913},
month = feb
}


@article{Richter:2009jc,
'''Liquid/Gas Flow Cell'''
author = {Richter, Claus-Peter and Shintani-Smith, Stephanie and Fishman, Andrew and David, Christian and Robinson, Ian and Rau, Christoph},
title = {{Imaging of cochlear tissue with a grating interferometer and hard X-rays}},
journal = {Microscopy Research and Technique},
year = {2009},
volume = {72},
number = {12},
pages = {902--907},
month = dec
}


@article{Gryko:2007p11880,
A small liquid flow cell is available with a peristaltic pump.  A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam.  The same cell is often used for room temperature gas flow experiments.
author = {Gryko, Piotr and Liang, Meng and Harder, Ross and Robinson, Ian K},
title = {{Observation of interference effects in coherent diffraction of nanocrystals under X-ray standing-wave illumination}},
journal = {Journal of Synchrotron Radiation},
year = {2007},
volume = {14},
number = {6},
pages = {471--476},
month = jan
}


@article{Hruszkewycz:2010p14757,
[[File:liquidcell1.jpg|320px]]
author = {Hruszkewycz, S O and Harder, R and Xiao, X and Fuoss, P H},
title = {{The effect of exit beam phase aberrations on parallel beam coherent x-ray reconstructions}},
journal = {Review of Scientific Instruments},
year = {2010},
volume = {81},
number = {12},
pages = {123706}
}


@article{Yang:2013dc,
'''Gas Exhaust'''
author = {Yang, Wenge and Huang, Xiaojing and Harder, Ross and Clark, Jesse N and Robinson, Ian K and Mao, Ho-kwang},
title = {{Coherent diffraction imaging of nanoscale strain evolution in a single crystal under high pressure}},
journal = {Nature Communications},
year = {2013},
volume = {4},
pages = {1680--},
month = apr
}


@article{markthesis,
A dedicated exhaust is available in 34-ID-C for experiments involving toxic or flammable gasses.  The flow rate was measured to be 70 cfm (1982 lpm). 
author = {Pfiefer, Mark},
title = {{MarkPfiefer_Thesis}},
journal = {Mark_thesis}
}


@article{Anonymous:2012p20141,
author = {Boragno, C and Buatier de Mongeot, F and Felici, R and Robinson, I},
title = {{Critical thickness for the agglomeration of thin metal films}},
journal = {Physical Review B},
year = {2009},
volume = {79},
number = {15},
pages = {155443},
month = apr
}


@article{Zhang:2013iz,
[[File:exhaust718.jpeg|320px]]
author = {Zhang, Fucai and Peterson, Isaac and Vila-Comamala, Joan and Diaz, Ana and Berenguer, Felisa and Bean, Richard and Chen, Bo and Menzel, Andreas and Robinson, Ian K and Rodenburg, John M},
title = {{Translation position determination in ptychographic coherent diffraction imaging}},
journal = {Opt. Express},
year = {2013},
volume = {21},
number = {11},
pages = {13592--13606}
}


@article{Vartanyants:2005p20140,
'''Coin Cell holder'''
author = {Vartanyants, I and Robinson, I and Onken, J and Pfeifer, M and williams, G and Pfeiffer, F and Metzger, H and Zhong, Z and Bauer, G},
title = {{Coherent x-ray diffraction from quantum dots}},
journal = {Physical Review B},
year = {2005},
volume = {71},
number = {24},
pages = {245302},
month = jun
}


@article{Huang:2013ip,
In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.  One can also be trained to load AMPIX cells in the echem lab.  34-ID-C also has an AMPIX cell holder compatible with the beamline.
author = {Huang, Xiaojing and Yan, Hanfei and Nazaretski, Evgeny and Conley, Raymond and Bouet, Nathalie and Zhou, Juan and Lauer, Kenneth and Li, Li and Eom, Daejin and Legnini, Daniel and Harder, Ross and Robinson, Ian K and Chu, Yong S},
title = {{11 nm hard X-ray focus from a large-aperture multilayer Laue lens}},
journal = {Scientific reports},
year = {2013},
volume = {3},
pages = {--},
month = dec
}


@article{Leake:2010p394,
[[File:coincell1.jpg|320px]]  [[File:coincell2.jpg|240px]]  [[File:Echemlab.png|150px]]
author = {Leake, S J},
title = {{Leake_PhDthesis}},
journal = {LeakeThesis},
year = {2010},
volume = {1},
number = {1},
pages = {1--277}
}


@article{Fohtung:2012p20917,
== Available Detectors (resident at the beamline) ==
author = {Fohtung, E and Kim, J W and Chan, Keith T and Harder, Ross and Fullerton, Eric E and Shpyrko, O G},
title = {{Probing the three-dimensional strain inhomogeneity and equilibrium elastic properties of single crystal Ni nanowires}},
journal = {Applied Physics Letters},
year = {2012},
volume = {101},
number = {3},
pages = {033107}
}


@article{Williams:2005tv,
'''ASI Quad (512x512) Timpix with GaAs absorber.'''
author = {Williams, Garth J},
title = {{Garth_small_thesis}},
year = {2005},
pages = {1--226},
month = nov
}


@article{Clark:2013uw,
This detector is our daily workhorse.  The structure of the GaAs needs to be divided out of the data.  We have a collection of whitefield images taken at various energies.  The pixels are 55 um, can run at about 100 Hz with 11,800 ph/pixel/read.
author = {Clark, J N and Beitra, L and Xiong, G and Higginbotham, A and Fritz, D M and Lemke, H T and Zhu, D and Chollet, M and Williams, G J and Messerschmidt, M and Abbey, B and Harder, R J and Korsunsky, A M and Wark, J S and Robinson, I K},
title = {{Ultrafast Three-Dimensional Imaging of Lattice Dynamics in Individual Gold Nanocrystals}},
journal = {Science},
year = {2013},
volume = {341},
number = {6141},
pages = {56--59},
month = jan,
annote = {10.1126/science.1236034


10.1126/science.1236034
[[File:ASItimepixGaAs.jpg|320px]]


10.1126/science.1236034}
}


@article{Boutet:2005wh,
author = {Boutet, S{\'e}bastien},
title = {{Boutet_thesis_low_res}},
year = {2005},
pages = {1--143},
month = nov
}


@article{Vartanyants:2001im,
'''ASI Single (256x256) Timepix with Si sensor'''
author = {Vartanyants, I A and Robinson, I K},
 
title = {{Partial coherence effects on the imaging of small crystals using coherent x-ray diffraction}},
The first PAD used routinely at the beamline until 2017. It's still available if a second detector is required for an experiment or the Quad fails for some reason. It can run at similar speeds to the Quad detector but has radiation damage limitations.
journal = {J. Phys.: Condens. Matter},
 
year = {2001},
[[File:ASItimepixSiSingle.jpg|240px]]
volume = {13},
 
number = {47},
 
pages = {10593--10611},
 
month = nov
'''Roper/PI direct detection CCD'''
}
 
@article{Mirarefi:2010je,
This was our workhorse for the first decade of the beamline.  It's now used primarily for recording powder rings from battery samples during cycling.  1340x1300 with 22.5 um pixels.  Runs at about 1 Hz or less reading full chip.  ROI can be read faster.  We only use this for CXD if we need the smaller pixels and larger area than the Andor.
author = {Mirarefi, Amir Y and Boutet, S{\'e}bastien and Ramakrishnan, Subramanian and Kiss, Andor J and Cheng, Chi-Hing C and DeVries, Arthur L and Robinson, Ian K and Zukoski, Charles F},
 
title = {{Small-angle X-ray scattering studies of the intact eye lens: Effect of crystallin composition and concentration on microstructure}},
[[File:PIccd1.jpg|320px]]
journal = {Biochimica et Biophysica Acta (BBA) - General Subjects},
 
year = {2010},
 
volume = {1800},
 
number = {6},
'''Andor direct detect CCD''' 
pages = {556--564},
 
month = jun
Used for only a couple of years, this CCD was added to the beamline just when Timepix was being commercialized.  It's actually a very good CCD with low noise and relatively flat dark field background.  1024x1024 with 13 um pixels.  Can read at about 3 Hz.  Roughly 60 photon pixel depth at 9 keV.  If we need the small pixels this detector is a goto.
}
 
@article{Harder:2013bh,
[[File:Andorccd1.jpg|320px]]
author = {Harder, Ross and Robinson, Ian K},
 
title = {{Coherent X-Ray Diffraction Imaging of Morphology and Strain in Nanomaterials}},
 
journal = {JOM},
 
year = {2013},
'''[https://www.hitachi-hightech.com/hhs-us/product_detail/?pn=ana-vortex-60ex Vortex EX 60]'''
volume = {65},
 
number = {9},
Used for x-ray fluorescence this detector has recently been calibrated and can be mounted in various positions to monitor fluorescence from a sample or measure elemental composition.
pages = {1202--1207},
 
month = jul
== Available Detectors (Non-resident but on loan with scheduling) ==
}
 
@article{FavreNicolin:2010p6156,
Additionally, there are PADs available from the [https://www.aps.anl.gov/Detectors/Area-Detectors APS detector pool].  Including Pilatus, Eiger, ASI Medipix3 and many others.
author = {Favre-Nicolin, V and Mastropietro, F and Eymery, J and Camacho, D and Niquet, Y M and Borg, B M and Messing, M E and Wernersson, L-E and Algra, R E and Bakkers, E P A M and Metzger, T H and Harder, R and Robinson, I K},
 
title = {{Analysis of strain and stacking faults in single nanowires using Bragg coherent diffraction imaging}},
 
journal = {New Journal of Physics},
== Site Access ==
year = {2010},
 
volume = {12},
 
number = {3},
For 2022-2 User Run starting in May 31st. 2022
pages = {035013},
month = mar
APS Covid guidance can be found here: https://www.aps.anl.gov/Users-Information/Updates/Covid-Rule-Regulations
}
@article{Stadler:2007p5272,
1. ESAFs which require Non-ANL Onsite Users: '''Must be submitted 14 days before the ESAF start date.'''  Any ESAF submitted after this date will be declined and we will ask them to reschedule or see if they can change to remote
author = {Stadler, Lorenz-M and Harder, Ross and Robinson, Ian and Rentenberger, Christian and Karnthaler, H Peter and Sepiol, Bogdan and Vogl, Gero},
 
title = {{Coherent x-ray diffraction imaging of grown-in antiphase boundaries in  FeAl}},
2. ESAFs with Remote or Mail-in Users only.  '''Must be submitted 7 days before the ESAF start date'''
journal = {Physical Review B},
 
year = {2007},
3. Argonne Onsite Users: '''ESAFS must be submitted 7 days before the ESAF start date.'''  If there is a mix of Non-ANL and ANL onsite users, ESAF must be submitted 14 days in advance.
volume = {76},
 
number = {1},
4. APS will be allowing for the 2022-2 run, 5 Onsite Users per ESAF.  If 6 or more onsite users are required then an onsite request form must be submitted for APS approval at the time of ESAF submission.  [https://www.aps.anl.gov/form/on-site-user-request-form '''User Justification Form''']
pages = {014204}
}
Remote/Mail-in ESAFS
@article{BerenguerdelaCuesta:2009kh,
 
author = {Berenguer de la Cuesta, F and Wenger, M P E and Bean, R J and Bozec, L and Horton, M A and Robinson, I K},
1. Remote site access for each remote user must be current for the experiment time frame.  If it is RED in the Experimenters tab then they will have to update their registrations in the APS User database: See link below
title = {{Coherent X-ray diffraction from collagenous soft tissues}},
https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page
journal = {Proceedings of the National Academy of Sciences},
year = {2009},
This should be done ASAP to allow for foreign nationals to get FAVOR approval.  It will take over a week to go through the approval process for foreign nationals so please encourage them to update their registration as soon as possible.
volume = {106},
number = {36},
All questions about site access should be sent to the APS User Office: [email protected]
pages = {15297--15301},
month = sep
Remote Users must be current in ESH223U Cybersecurity.  This is an online course that can be completed via the link below:
}
https://beam.aps.anl.gov/pls/apsweb/rt0004.intro_process
@article{Boutet:2008dv,
Because the remote user is not coming onsite we require completion of ESH223U Cybersecurity before ESAF Approval.
author = {Boutet, S and Robinson, I K},
 
title = {{Coherent X-ray diffractive imaging of protein crystals}},
ESAFS will not be approved if the Remote User does not have site access or completed ESH223U (see below)
journal = {Journal of Synchrotron Radiation},
year = {2008},
1. Mail-In users.  Mail-in site access must be current for the experiment time frame.  ESAF system has been modified so that the Mail-in users are no longer greyed out for their site access.  If they are expired in their site access it will also be in BOLD and RED.  Moving forward we will ask Mail-in Users to update their APS registration using the link provided.
volume = {15},
number = {6},
https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page
pages = {576--583},
month = nov
All questions about site access should be sent to the APS User Office: apsuser@anl.gov
}
@article{Robinson:2001ix,
ESAFS will not be approved if Mail-In users do not have active site access during their experiment time.   
author = {Robinson, I K and Vartanyants, I A},
title = {{Use of coherent X-ray diffraction to map strain fields in nanocrystals}},
Onsite Users
journal = {Applied Surface Science},
1. Onsite Site access for each onsite user must be current for the experiment time frame.  If it is RED in the Experimenters tab then they will have to update their registrations in the APS database:
year = {2001},
https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page
volume = {182},
number = {3-4},
This should be done ASAP to allow for foreign nationals to get FAVOR approval. 
pages = {186--191},
 
month = oct
ESAFS will not be approved if the Onsite User does not have site access. Gate passes will not be granted if the ESAF is not approved
}
@article{Robinson:2003hj,
1. Training: Training for all onsite users can be done before arrival to the APS at the remote training link:
author = {Robinson, I K and Kenney-Benson, C A and Vartanyants, I A},
https://beam.aps.anl.gov/pls/apsweb/rt0004.intro_process
title = {{Sources of decoherence in beamline optics}},
journal = {Physica B: Condensed Matter},
COVID 100 is no longer required for onsite users.
year = {2003},
Sector orientation will be completed once onsite.
volume = {336},
Additional classes can be found on the remote training link or contact the APS User Office [email protected]
number = {1-2},
pages = {56--62},
Please let me know if you have any questions.
month = aug
}
Nena Moonier
@article{Beitra:2010p15094,
APS Safety Officer
author = {Beitra, Loren and Watari, Moyu and Matsuura, Takashi and Shimamoto, Naonobu and Harder, Ross and Robinson, Ian},
title = {{Confocal Microscope Alignment of Nanocrystals for Coherent Diffraction Imaging}},
journal = {AIP Conference Proceedings},
year = {2010},
volume = {1234},
number = {1},
pages = {57--60}
}
@article{Vartanyants:2003br,
author = {Vartanyants, I A and Robinson, I K},
title = {{Origins of decoherence in coherent X-ray diffraction experiments}},
journal = {Optics Communications},
year = {2003},
volume = {222},
number = {1-6},
pages = {29--50},
month = jul
}
@incollection{Harder:2012bz,
author = {Harder, Ross},
title = {{Coherent Diffraction Imaging of Strain on the Nanoscale}},
booktitle = {Characterization of Materials},
year = {2012},
publisher = {John Wiley {\&} Sons, Inc.}
}
@article{Clark:2012p22298,
author = {Clark, J N and Huang, X and Harder, R and Robinson, I K},
title = {{High-resolution three-dimensional partially coherent diffraction imaging}},
journal = {Nature Communications},
year = {2012},
volume = {3},
pages = {993--},
month = aug
}
@article{Huang:2012p22048,
author = {Huang, Xiaojing and Harder, Ross and Leake, Steven and Clark, Jesse and Robinson, Ian},
title = {{Three-dimensional Bragg coherent diffraction imaging of an extended ZnO crystalThis article also forms part of a special issue dedicated to advanced diffraction imaging methods of materials, which will be published as a virtual special issue of the journal in 2012/2013.}},
journal = {Journal of applied crystallography},
year = {2012},
volume = {45},
number = {4},
pages = {778--784},
month = jun,
annote = {doi:10.1107/S0021889812018900}
}
@article{Williams:2003p19351,
author = {williams, G and Pfeifer, M and Vartanyants, I and Robinson, I},
title = {{Three-Dimensional Imaging of Microstructure in Au Nanocrystals}},
journal = {Physical review letters},
year = {2003},
volume = {90},
number = {17},
pages = {175501},
month = apr
}
</bibtex>

Latest revision as of 21:34, 26 March 2024

Apply for beamtime at 34-ID-C

APS Users Information

Publications

Our current publication list

Setup Images and Drawings

Media: 34IDC_basic_instrument_diagrams_2022.pdf

Specs:

The detector arm can move in two dimensions.

Delta: -2 -> 45 degrees

Gamma: -2 -> 150 degrees

Delta is the axis perpendicular to the floor, essentially moves the detector horizontally. The range of Delta is -2 to 45 degrees. Although it can be a little larger if the other detector axis is increased. Gamma is the axis parallel to the floor. It effectively moves the detector up and down. The range is dependent on the configuration of the instrument. It can be as much as 150 degrees.

Sample Environments (Resident at beamline)

Current Gas Inventory

Updated every few weeks. 34-ID-C gases in stock

Kinematic Sample Mount

The typical sample mount for STP measurements in air is a Thorlabs KBT1x1 magnetic kinematic mount. The usual fixation method is double sided sticky tape, though wax and nail polish are available.

Kinematicsamplemount.jpg


Heater Cell

The heater cell is capable of several hundred degrees centigrade. Improvements are underway to reach up to 1000 C. It also supports gas flow through the chamber. It is not vacuum compatible.

Heater1.jpg Heater2.jpg



Linkam Cryo stage

The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber includes a magnetically secured removable cover.

Linkam1.JPG Linkam2.jpg



Liquid/Gas Flow Cell

A small liquid flow cell is available with a peristaltic pump. A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam. The same cell is often used for room temperature gas flow experiments.

Liquidcell1.jpg

Gas Exhaust

A dedicated exhaust is available in 34-ID-C for experiments involving toxic or flammable gasses. The flow rate was measured to be 70 cfm (1982 lpm).


Exhaust718.jpeg

Coin Cell holder

In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS. One can also be trained to load AMPIX cells in the echem lab. 34-ID-C also has an AMPIX cell holder compatible with the beamline.

Coincell1.jpg Coincell2.jpg Echemlab.png

Available Detectors (resident at the beamline)

ASI Quad (512x512) Timpix with GaAs absorber.

This detector is our daily workhorse. The structure of the GaAs needs to be divided out of the data. We have a collection of whitefield images taken at various energies. The pixels are 55 um, can run at about 100 Hz with 11,800 ph/pixel/read.

ASItimepixGaAs.jpg


ASI Single (256x256) Timepix with Si sensor

The first PAD used routinely at the beamline until 2017. It's still available if a second detector is required for an experiment or the Quad fails for some reason. It can run at similar speeds to the Quad detector but has radiation damage limitations.

ASItimepixSiSingle.jpg


Roper/PI direct detection CCD

This was our workhorse for the first decade of the beamline. It's now used primarily for recording powder rings from battery samples during cycling. 1340x1300 with 22.5 um pixels. Runs at about 1 Hz or less reading full chip. ROI can be read faster. We only use this for CXD if we need the smaller pixels and larger area than the Andor.

PIccd1.jpg


Andor direct detect CCD

Used for only a couple of years, this CCD was added to the beamline just when Timepix was being commercialized. It's actually a very good CCD with low noise and relatively flat dark field background. 1024x1024 with 13 um pixels. Can read at about 3 Hz. Roughly 60 photon pixel depth at 9 keV. If we need the small pixels this detector is a goto.

Andorccd1.jpg


Vortex EX 60

Used for x-ray fluorescence this detector has recently been calibrated and can be mounted in various positions to monitor fluorescence from a sample or measure elemental composition.

Available Detectors (Non-resident but on loan with scheduling)

Additionally, there are PADs available from the APS detector pool. Including Pilatus, Eiger, ASI Medipix3 and many others.


Site Access

For 2022-2 User Run starting in May 31st. 2022

APS Covid guidance can be found here: https://www.aps.anl.gov/Users-Information/Updates/Covid-Rule-Regulations

1. ESAFs which require Non-ANL Onsite Users: Must be submitted 14 days before the ESAF start date. Any ESAF submitted after this date will be declined and we will ask them to reschedule or see if they can change to remote

2. ESAFs with Remote or Mail-in Users only. Must be submitted 7 days before the ESAF start date

3. Argonne Onsite Users: ESAFS must be submitted 7 days before the ESAF start date. If there is a mix of Non-ANL and ANL onsite users, ESAF must be submitted 14 days in advance.

4. APS will be allowing for the 2022-2 run, 5 Onsite Users per ESAF. If 6 or more onsite users are required then an onsite request form must be submitted for APS approval at the time of ESAF submission. User Justification Form

Remote/Mail-in ESAFS

1. Remote site access for each remote user must be current for the experiment time frame. If it is RED in the Experimenters tab then they will have to update their registrations in the APS User database: See link below https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page

This should be done ASAP to allow for foreign nationals to get FAVOR approval. It will take over a week to go through the approval process for foreign nationals so please encourage them to update their registration as soon as possible.

All questions about site access should be sent to the APS User Office: [email protected]

Remote Users must be current in ESH223U Cybersecurity. This is an online course that can be completed via the link below: https://beam.aps.anl.gov/pls/apsweb/rt0004.intro_process Because the remote user is not coming onsite we require completion of ESH223U Cybersecurity before ESAF Approval.

ESAFS will not be approved if the Remote User does not have site access or completed ESH223U (see below)

1. Mail-In users. Mail-in site access must be current for the experiment time frame. ESAF system has been modified so that the Mail-in users are no longer greyed out for their site access. If they are expired in their site access it will also be in BOLD and RED. Moving forward we will ask Mail-in Users to update their APS registration using the link provided.

https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page

All questions about site access should be sent to the APS User Office: [email protected]

ESAFS will not be approved if Mail-In users do not have active site access during their experiment time.

Onsite Users 1. Onsite Site access for each onsite user must be current for the experiment time frame. If it is RED in the Experimenters tab then they will have to update their registrations in the APS database: https://beam.aps.anl.gov/pls/apsweb/ufr_main_pkg.usr_start_page

This should be done ASAP to allow for foreign nationals to get FAVOR approval.

ESAFS will not be approved if the Onsite User does not have site access. Gate passes will not be granted if the ESAF is not approved

1. Training: Training for all onsite users can be done before arrival to the APS at the remote training link: https://beam.aps.anl.gov/pls/apsweb/rt0004.intro_process

COVID 100 is no longer required for onsite users. Sector orientation will be completed once onsite. Additional classes can be found on the remote training link or contact the APS User Office [email protected]

Please let me know if you have any questions.

Nena Moonier APS Safety Officer