Difference between revisions of "34-ID-C"
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The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber, than that pictured, includes a magnetically secured removable cover. | The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber, than that pictured, includes a magnetically secured removable cover. | ||
[[File:Linkam1.JPG|320px]] | [[File:Linkam1.JPG|320px]] [[File:Linkam2.jpg|320px]] | ||
'''Liquid/Gas Flow Cell''' | '''Liquid/Gas Flow Cell''' | ||
Revision as of 19:53, 24 February 2018
Setup Images and Drawings
Media: 34IDC_basic_instrument_diagrams_for_mounting_assistance_etc.pdf
Sample Environments (Resident at beamline)
Heater Cell
The heater cell is capable of several hundred degrees centigrade. Improvements are underway to reach up to 1000 C. It also supports a single gas flow through the chamber. It is not vacuum compatible.
Linkam Cryo stage
The guts of this cell is a Linkam THMS controller. Temperatures as low as -100 C are possible but since the 3D printed chamber is not vacuum compatible, icing can be significant. Development of a highly dried gas environment is underway to minimize icing. The cell can also support moderate heating, limited by melting the 3D printed chamber. We have maintained 50 C for many hours with no problem. A newer version of the chamber, than that pictured, includes a magnetically secured removable cover.
Liquid/Gas Flow Cell
A small liquid flow cell is available with a peristaltic pump. A mylar or propylene film is pressed over the sample to maintain a thin liquid layer to minimize absorption of the x-ray beam. The same cell is often used for room temperature gas flow experiments.
Coin Cell holder
In-situ battery cycling is possible with a potentiostat that can be borrowed from the electrochemistry lab at APS.
Available Detectors
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